1BOY
EXTRACELLULAR REGION OF HUMAN TISSUE FACTOR
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-6A |
| Synchrotron site | Photon Factory |
| Beamline | BL-6A |
| Detector technology | IMAGE PLATE |
| Collection date | 1994-03 |
| Detector | FUJI |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 45.400, 45.400, 230.800 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.200 |
| R-factor | 0.203 |
| Rwork | 0.203 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.980 |
| Data reduction software | DENZO (/ SCALEPACK) |
| Data scaling software | SCALEPACK |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.200 * |
| Rmerge | 0.065 |
| Number of reflections | 12666 |
| Completeness [%] | 96.0 |
| Redundancy | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7.5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 5.0 (mg/ml) | |
| 2 | 1 | reservoir | HEPES | 0.1 (M) | |
| 3 | 1 | reservoir | ammonium sulfate | 2.6 (M) |
