1BMP
BONE MORPHOGENETIC PROTEIN-7
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1993-11-30 |
| Detector | RIGAKU |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 99.460, 99.460, 42.090 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 2.800 |
| R-factor | 0.227 * |
| Rwork | 0.227 |
| R-free | 0.30800 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.025 |
| Data reduction software | R-AXIS (SOFTWARE) |
| Data scaling software | R-AXIS |
| Phasing software | X-PLOR |
| Refinement software | PROFFT |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.800 * |
| Rmerge | 0.067 |
| Number of reflections | 5502 |
| Completeness [%] | 87.0 |
| Redundancy | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 5 * | 22 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 5 (mg/ml) | |
| 2 | 1 | drop | ammonium sulfate | 4 (%sat) | |
| 3 | 1 | drop | sodium acetate | 25 (mM) | |
| 4 | 1 | reservoir | ammonium sulfate | 8 (%sat) | |
| 5 | 1 | reservoir | sodium acetate | 50 (mM) |
