Experimental procedure
| Temperature [K] | 277 |
| Detector technology | IMAGE PLATE |
| Collection date | 1993-10-10 |
| Detector | RIGAKU RAXIS II |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.200, 85.900, 58.100 |
| Unit cell angles | 90.00, 109.30, 90.00 |
Refinement procedure
| Resolution | 28.000 - 1.800 |
| R-factor | 0.175 |
| Rwork | 0.175 |
| R-free | 0.20700 |
| Structure solution method | MIR |
| RMSD bond length | 0.013 |
| RMSD bond angle | 22.800 * |
| Data reduction software | R-AXIS |
| Data scaling software | R-AXIS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.000 | 1.900 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.043 | |
| Total number of observations | 117092 * | |
| Number of reflections | 36163 | |
| Completeness [%] | 82.0 | 40.7 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, sitting drop * | 7 | pH 7.0 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | PEG6000 | 30 (%) | |
| 2 | 1 | reservoir | HEPES | 0.1 (M) |
