1BD4
UPRT-URACIL COMPLEX
Experimental procedure
Temperature [K] | 298 |
Collection date | 1997-01 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.390, 141.770, 71.460 |
Unit cell angles | 90.00, 114.82, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.200 |
R-factor | 0.181 * |
Rwork | 0.194 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.903 |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 * | |
High resolution limit [Å] | 2.200 | 2.160 * |
Rmerge | 0.052 * | |
Total number of observations | 111427 * | |
Number of reflections | 53303 * | |
Completeness [%] | 87.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | Tris-HCl | 10 (mM) | |
2 | 1 | drop | dithiothreitol | 10 (mM) | |
3 | 1 | drop | protein | 25-40 (mg/ml) | |
4 | 1 | reservoir | ammonium phosphate | 1.0 (M) | |
5 | 1 | reservoir | citrate | 0.1 (M) | |
6 | 1 | reservoir | 0.2 (M) |