1AZR

CRYSTAL STRUCTURE OF PSEUDOMONAS AERUGINOSA ZINC AZURIN MUTANT ASP47ASP AT 2.4 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	57.810, 81.530, 112.610
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 * - 2.400
R-factor	0.171 *
Rwork	0.171
RMSD bond length	0.016
RMSD bond angle	2.900 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.400 *
Rmerge	0.066 *
Total number of observations	80786 *
Number of reflections	17198 *
Completeness [%]	83.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *	5.7 *	297-298 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1		ammonium sulfate	3.6 (M)
2	1		lithium nitrate	0.5 (M)
3	1		acetate	0.1 (M)