1AV5
PKCI-SUBSTRATE ANALOG
Experimental procedure
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1996-10-17 |
Detector | RIGAKU RAXIS II |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.200, 77.800, 80.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.000 |
R-factor | 0.229 |
Rwork | 0.229 |
R-free | 0.27900 |
RMSD bond length | 0.020 |
RMSD bond angle | 25.557 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.056 |
Total number of observations | 194693 * |
Number of reflections | 26213 * |
Completeness [%] | 71.5 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.5 | 20 * | Lima, C.D., (1996) Proc.Nat.Acad.Sci.USA, 93, 5357. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 13-18 (%) | |
2 | 1 | reservoir | sodium cacodylate | 100 (mM) | |
3 | 1 | drop | PKCI-1 | 3-6 (mg/ml) |