1ATZ
HUMAN VON WILLEBRAND FACTOR A3 DOMAIN
Experimental procedure
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-06 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 35.200, 98.520, 44.580 |
Unit cell angles | 90.00, 90.64, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.800 |
R-factor | 0.174 |
Rwork | 0.174 |
R-free | 0.24000 |
Structure solution method | MAD |
RMSD bond length | 0.009 |
RMSD bond angle | 24.000 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | X-PLOR (3.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.880 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.048 | 0.059 |
Number of reflections | 28127 | |
<I/σ(I)> | 43.8 | 29.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.2 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8.5 | used to seeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | sodium acetate | 200 (mM) | |
2 | 1 | reservoir | Tris-HCl | 0.1 (M) | |
3 | 1 | reservoir | PEG3000 | 30 (%(w/v)) |