Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1ARW

CRYSTAL STRUCTURES OF CYANIDE-AND TRIIODIDE-BOUND FORMS OF ARTHROMYCES RAMOSUS PEROXIDASE AT DIFFERENT PH VALUES. PERTURBATIONS OF ACTIVE SITE RESIDUES AND THEIR IMPLICATION IN ENZYME CATALYSIS

Experimental procedure
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-6A
Synchrotron sitePhoton Factory
BeamlineBL-6A
Detector technologyDIFFRACTOMETER
DetectorWEISSENBERG
Spacegroup nameP 42 21 2
Unit cell lengths74.570, 74.570, 117.470
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution7.000 - 1.600
R-factor0.185
Rwork0.185
RMSD bond length0.019
RMSD bond angle0.052

*

Phasing softwareX-PLOR
Refinement softwareX-PLOR
Data quality characteristics
 Overall
High resolution limit [Å]1.600

*

Rmerge0.071

*

Total number of observations158600

*

Number of reflections37412

*

Completeness [%]84.5

*

Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

*

424

*

seeding

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropARP20-40 (M)
21reservoirammonium sulfate32 (%sat)
31reservoirTris-HCl20 (mM)

219869

PDB entries from 2024-05-15

PDB statisticsPDBj update infoContact PDBjnumon