1ARG

Aspartate aminotransferase, phospho-5'-pyridoxyl aspartate complex

Experimental procedure

Temperature [K]	277
Detector technology	IMAGE PLATE
Collection date	1994-02-21
Detector	MARRESEARCH
Spacegroup name	P 1 21 1
Unit cell lengths	85.390, 78.950, 89.290
Unit cell angles	90.00, 118.54, 90.00

Refinement procedure

Resolution	8.000 - 2.200
R-factor	0.198
RMSD bond length	0.011
RMSD bond angle	25.000 *
Data reduction software	XDS
Refinement software	TNT (4C)

Data quality characteristics

	Overall
Low resolution limit [Å]	40.000 *
High resolution limit [Å]	2.200 *
Rmerge	0.057
Number of reflections	44764 *
Completeness [%]	93.0 *
Redundancy	3.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.5	4 *	pH 7.5