1APV

CRYSTALLOGRAPHIC ANALYSIS OF TRANSITION STATE MIMICS BOUND TO PENICILLOPEPSIN: DIFLUOROSTATINE-AND DIFLUOROSTATONE-CONTAINING PEPTIDES

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	97.520, 46.570, 66.230
Unit cell angles	90.00, 116.03, 90.00

Refinement procedure

Resolution	8.000 - 1.800
R-factor	0.131
RMSD bond length	0.017
RMSD bond angle	0.038 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	45.000 *
High resolution limit [Å]	1.800 *
Rmerge	0.037 *
Number of reflections	24854 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *			NMR *