1AN0
CDC42HS-GDP COMPLEX
Experimental procedure
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F2 |
Synchrotron site | CHESS |
Beamline | F2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1996-12 |
Detector | PRINCETON 2K |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 99.440, 99.440, 102.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.800 |
R-factor | 0.228 |
Rwork | 0.228 |
R-free | 0.34400 |
Structure solution method | MAD PHASING |
RMSD bond length | 0.009 |
RMSD bond angle | 1.857 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASES (V. 95) |
Refinement software | XTALVIEW |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.047 | 0.178 |
Number of reflections | 12366 | |
<I/σ(I)> | 4831.3 | 592.5 |
Completeness [%] | 86.4 | 67.2 |
Redundancy | 3.11 | 1.93 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.8 | pH 4.8 |