1AN0
CDC42HS-GDP COMPLEX
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F2 |
| Synchrotron site | CHESS |
| Beamline | F2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1996-12 |
| Detector | PRINCETON 2K |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 99.440, 99.440, 102.670 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.800 |
| R-factor | 0.228 |
| Rwork | 0.228 |
| R-free | 0.34400 |
| Structure solution method | MAD PHASING |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.857 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | PHASES (V. 95) |
| Refinement software | XTALVIEW |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.900 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.047 | 0.178 |
| Number of reflections | 12366 | |
| <I/σ(I)> | 4831.3 | 592.5 |
| Completeness [%] | 86.4 | 67.2 |
| Redundancy | 3.11 | 1.93 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.8 | pH 4.8 |
