1ALD
ACTIVITY AND SPECIFICITY OF HUMAN ALDOLASES
Experimental procedure
| Spacegroup name | P 64 2 2 |
| Unit cell lengths | 96.340, 96.340, 167.000 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 3.000 * - 2.000 |
| R-factor | 0.22 * |
| Rwork | 0.220 |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.000 * |
| Number of reflections | 21427 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | 7.3 * | referred to 'Eagles, P. A.', (1969) J. Mol. Biol., 45, 533-544 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | protein | 5 (mg/ml) | |
| 2 | 1 | 1 | triethanolamine-hydrochloride | 0.1 (M) | |
| 3 | 1 | 1 | EDTA | 5 (mM) | |
| 4 | 1 | 1 | ammonium sulfate | 44-49 (%sat) |
