1ADV

EARLY E2A DNA-BINDING PROTEIN

Experimental procedure

Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	1994-05-10
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	61.370, 89.580, 149.770
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 3.200
R-factor	0.206
Rwork	0.206
R-free	0.33600
RMSD bond length	0.007
RMSD bond angle	24.200 *
Data reduction software	XDS
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	25.000
High resolution limit [Å]	3.200	3.200 *
Rmerge	0.083	0.236 *
Total number of observations	42619 *
Number of reflections	13965
Completeness [%]	98.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	0.5 (%)
2	1	reservoir	ammonium sulfate	13 (%sat)