1AAC
AMICYANIN OXIDIZED, 1.31 ANGSTROMS
Experimental procedure
| Detector technology | AREA DETECTOR |
| Collection date | 1991-06-20 |
| Detector | XUONG-HAMLIN MULTIWIRE |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 28.950, 56.540, 27.550 |
| Unit cell angles | 90.00, 96.38, 90.00 |
Refinement procedure
| Resolution | 8.000 - 1.310 |
| R-factor | 0.155 |
| Rwork | 0.155 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 2.520 |
| Data reduction software | SDMS |
| Phasing software | X-PLOR (2.1) |
| Refinement software | X-PLOR (2.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.160 |
| High resolution limit [Å] | 1.310 |
| Rmerge | 0.050 |
| Total number of observations | 199399 * |
| Number of reflections | 21219 |
| Completeness [%] | 99.0 |
| Redundancy | 5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | phosphate | 3.0 (M) | |
| 2 | 1 | reservoir | ammonium sulfate |
