1A7E
HYDROXOMET MYOHEMERYTHRIN FROM THEMISTE ZOSTERICOLA
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 119 |
Detector technology | IMAGE PLATE |
Collection date | 1988-08 |
Detector | RIGAKU |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.885, 81.170, 36.685 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.800 |
R-factor | 0.186 |
Rwork | 0.186 |
R-free | 0.22700 |
RMSD bond length | 0.017 |
RMSD bond angle | 20.200 * |
Data reduction software | R-AXIS |
Data scaling software | R-AXIS |
Phasing software | X-PLOR (3.8) |
Refinement software | X-PLOR (3.8) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | |
High resolution limit [Å] | 1.740 | 1.740 * |
Rmerge | 0.070 | |
Total number of observations | 102018 * | |
Number of reflections | 11853 | |
Completeness [%] | 88.2 | 49.6 * |
Redundancy | 8.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 * | 27% PEG 6K, 100MM HEPES, 1.0M LICL (PH 7.0) |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG6000 | 27 (%(v/v)) | |
2 | 1 | reservoir | HEPES | 0.1 (M) | |
3 | 1 | reservoir | 1.0 (M) | pH7.0 | |
4 | 1 | drop | Tris-HCl | 0.05 (M) | |
5 | 1 | drop | 0.2 (M) | pH8.0 |