1A6U
B1-8 FV FRAGMENT
Experimental procedure
| Temperature [K] | 269 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-08 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 72.030, 85.780, 37.420 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.000 - 2.100 |
| Rwork | 0.192 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1mfa |
| RMSD bond length | 0.020 |
| RMSD bond angle | 0.058 |
| Data reduction software | MOSFLM |
| Data scaling software | Agrovata |
| Phasing software | CCP4 ((ALMN)) |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 13.700 | 2.050 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.054 | 0.177 |
| Number of reflections | 105196 | |
| Completeness [%] | 92.3 | 61.2 |
| Redundancy | 4.3 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | CRYSTALS WERE GROWN USING AMMONIUM SULFATE AS PRECIPITANT. |
