Experimental procedure
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX7.2 |
| Synchrotron site | SRS |
| Beamline | PX7.2 |
| Temperature [K] | 300 |
| Detector technology | FILM |
| Collection date | 1983-06 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 35.100, 46.200, 186.200 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.300 |
| R-factor | 0.186 |
| Rwork | 0.186 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4gcr |
| RMSD bond length | 0.012 |
| RMSD bond angle | 27.300 * |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((AGROVATA) |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 24.000 |
| High resolution limit [Å] | 2.300 |
| Rmerge | 0.104 |
| Number of reflections | 6300 |
| Completeness [%] | 88.7 |
| Redundancy | 4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 6.86 * | pH 7.0 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | PEG6000 | 13 (%(w/v)) | |
| 2 | 1 | drop | sodium phosphate | 0.05 (M) |
