187D
HYDRATION PATTERNS AND INTERMOLECULAR INTERACTIONS IN A-DNA CRYSTAL STRUCTURES. IMPLICATIONS FOR DNA RECOGNITION
Experimental procedure
| Temperature [K] | 288 |
| Detector technology | DIFFRACTOMETER |
| Detector | NICOLET |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 43.360, 43.360, 24.830 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.250 |
| R-factor | 0.134 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.019 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.250 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7 | Wang, A. H.-J., (1982) Proc. Nat. Acad. Sci. USA., 79, 3968. * |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | MPD | ||
| 3 | 1 | 1 | NA CACODYLATE | ||
| 4 | 1 | 1 | SPERMINE | ||
| 5 | 1 | 1 | MGCL2 | ||
| 6 | 1 | 2 | WATER | ||
| 7 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | sodium cacodylate | 25 (mM) | ||
| 2 | 1 | spermine | 0.6 (mM) | ||
| 4 | 1 | octamer | 1.2 (mM) | ||
| 5 | 1 | 2 | MPD | 30 (%) |
