180D
SEQUENCE-DEPENDENT MICROHETEROGENEITY OF Z-DNA: THE CRYSTAL AND MOLECULAR STRUCTURES OF D(CACGCG).D(CGCGTG) AND D(CGCACG).D(CGTGCG)
Experimental procedure
Temperature [K] | 296 |
Detector technology | DIFFRACTOMETER |
Detector | ENRAF-NONIUS CAD4 |
Spacegroup name | P 1 1 21 |
Unit cell lengths | 17.750, 17.760, 42.770 |
Unit cell angles | 90.00, 90.00, 120.05 |
Refinement procedure
Resolution | 10.000 - 2.500 |
R-factor | 0.161 |
RMSD bond length | 0.071 |
RMSD bond angle | 0.070 |
Refinement software | NUCLSQ |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | pH 6.80, VAPOR DIFFUSION, HANGING DROP |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | NA CACODYLATE | ||
3 | 1 | 1 | BACL2 | ||
4 | 1 | 2 | WATER | ||
5 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | duplex DNA | 1 (mM) | |
2 | 1 | drop | sodium cacodylate | 50 (mM) | |
3 | 1 | drop | 10 (mM) | ||
4 | 1 | reservoir | MPD | 25 (%) |