163L

CONTROL OF ENZYME ACTIVITY BY AN ENGINEERED DISULFIDE BOND

Experimental procedure

Spacegroup name	P 32 2 1
Unit cell lengths	60.850, 60.850, 97.020
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 1.800
R-factor	0.146
RMSD bond length	0.016
RMSD bond angle	2.000
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.024 *
Number of reflections	17920 *
Completeness [%]	88.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	other *			Eriksson, A.E., (1993) J. Mol. Biol., 229, 747., Nicholson, H., (1991) Biochemistry, 30, 9816. *