13DO

helloB-GGFFAA-A6Dpp+PFHpA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-G
Synchrotron site	APS
Beamline	21-ID-G
Temperature [K]	100
Detector technology	PIXEL
Collection date	2026-04-08
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.978720
Spacegroup name	C 1 2 1
Unit cell lengths	37.836, 9.154, 36.495
Unit cell angles	90.00, 110.10, 90.00

Refinement procedure

Resolution	18.600 - 1.140
R-factor	0.171
Rwork	0.167
R-free	0.21290
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.369
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	18.600	1.181
High resolution limit [Å]	1.140	1.140
Number of reflections	4559	422
<I/σ(I)>	18.35
Completeness [%]	99.1
Redundancy	5.7
CC(1/2)	0.999	0.992

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SLOW COOLING		298	Acetonitrile, water