12HP
Crystal structure of the CD7 ectodomain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2026-02-12 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1 |
| Spacegroup name | P 64 |
| Unit cell lengths | 106.420, 106.420, 151.040 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 39.340 - 2.000 |
| R-factor | 0.2819 |
| Rwork | 0.248 |
| R-free | 0.26790 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.085 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (2.0_5885) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.340 | 2.050 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.509 | |
| Rmeas | 0.546 | |
| Number of reflections | 65170 | 4821 |
| <I/σ(I)> | 8.86 | 2.97 |
| Completeness [%] | 99.8 | 99.7 |
| Redundancy | 6.8 | 7.6 |
| CC(1/2) | 0.996 | 0.959 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293.15 | 0.7M NaH2PO4, 0.7M KH2PO4, 0.075M HEPES (pH=7.5), 25% glycerol |
