温度: 298 K / 手法: 蒸気拡散法, ハンギングドロップ法 / pH: 5.1 詳細: 22% w/v PEG4K, 10 mM sodium acetate pH 5.1. Crystals of RNase A-AP-1 were formed by soaking pre-grown RNase A crystals for 3 h in a solution containing 5 mM AP-1 dissolved in DMSO and then added to the reservoir.
解像度: 2.15→72.94 Å / Cor.coef. Fo:Fc: 0.951 / Cor.coef. Fo:Fc free: 0.915 / SU B: 7.085 / SU ML: 0.177 / 交差検証法: THROUGHOUT / ESU R: 0.296 / ESU R Free: 0.226 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.25049
681
5.2 %
RANDOM
Rwork
0.18704
-
-
-
obs
0.1904
12526
99.5 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK