- PDB-4zfp: A new crystal structure for the adduct formed in the reaction bet... -
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基本情報
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データベース: PDB / ID: 4zfp
タイトル
A new crystal structure for the adduct formed in the reaction between AuSac2, a cytotoxic homoleptic gold(I) compound with the saccharinate ligand, and the model protein hen egg white lysozyme
温度: 298 K / 手法: 蒸気拡散法, ハンギングドロップ法 / pH: 4.4 詳細: Best crystals grow within 2 days from the following conditions: 0.6 M NaNO3, 0.1 M sodium acetate pH 4.4 and 20 % ethylene glycol. PH範囲: 4.4
解像度: 1.96→54.86 Å / Cor.coef. Fo:Fc: 0.965 / Cor.coef. Fo:Fc free: 0.933 / SU B: 5.169 / SU ML: 0.141 / 交差検証法: THROUGHOUT / ESU R: 0.205 / ESU R Free: 0.182 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.23501
386
4.6 %
RANDOM
Rwork
0.16974
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obs
0.17282
7942
97.22 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK