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- PDB-4xwo: Structure of Get3 bound to the transmembrane domain of Sec22 -

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Basic information

Entry
Database: PDB / ID: 4xwo
TitleStructure of Get3 bound to the transmembrane domain of Sec22
Components
  • ATPase GET3
  • Antibody heavy chain
  • Antibody light chain
  • Sec22
KeywordsHYDROLASE/TRANSPORT PROTEIN / membrane protein targeting complex / HYDROLASE-TRANSPORT PROTEIN complex
Function / homology
Function and homology information


GET complex / pheromone-dependent signal transduction involved in conjugation with cellular fusion / tail-anchored membrane protein insertion into ER membrane / Hydrolases; Acting on acid anhydrides / protein insertion into ER membrane / post-translational protein targeting to endoplasmic reticulum membrane / response to arsenic-containing substance / retrograde vesicle-mediated transport, Golgi to endoplasmic reticulum / response to metal ion / protein folding chaperone ...GET complex / pheromone-dependent signal transduction involved in conjugation with cellular fusion / tail-anchored membrane protein insertion into ER membrane / Hydrolases; Acting on acid anhydrides / protein insertion into ER membrane / post-translational protein targeting to endoplasmic reticulum membrane / response to arsenic-containing substance / retrograde vesicle-mediated transport, Golgi to endoplasmic reticulum / response to metal ion / protein folding chaperone / guanyl-nucleotide exchange factor activity / unfolded protein binding / response to heat / cellular response to oxidative stress / endoplasmic reticulum membrane / Golgi apparatus / endoplasmic reticulum / ATP hydrolysis activity / ATP binding / identical protein binding / metal ion binding / cytosol
Similarity search - Function
Arsenical pump ATPase, ArsA/GET3, eukaryotic / Arsenical pump ATPase, ArsA/GET3 / Anion-transporting ATPase-like domain / Anion-transporting ATPase / P-loop containing nucleotide triphosphate hydrolases / Immunoglobulins / Immunoglobulin-like / Sandwich / P-loop containing nucleoside triphosphate hydrolase / Rossmann fold ...Arsenical pump ATPase, ArsA/GET3, eukaryotic / Arsenical pump ATPase, ArsA/GET3 / Anion-transporting ATPase-like domain / Anion-transporting ATPase / P-loop containing nucleotide triphosphate hydrolases / Immunoglobulins / Immunoglobulin-like / Sandwich / P-loop containing nucleoside triphosphate hydrolase / Rossmann fold / 3-Layer(aba) Sandwich / Mainly Beta / Alpha Beta
Similarity search - Domain/homology
ADENOSINE-5'-DIPHOSPHATE / ADENOSINE-5'-TRIPHOSPHATE / ATPase GET3
Similarity search - Component
Biological speciesSaccharomyces cerevisiae (brewer's yeast)
HOMO SAPIENS (human)
synthetic construct (others)
MethodX-RAY DIFFRACTION / SYNCHROTRON / MOLECULAR REPLACEMENT / Resolution: 2.75 Å
AuthorsMateja, A. / Paduch, M. / Chang, H.-Y. / Szydlowska, A. / Kossiakoff, A.A. / Hegde, R.S. / Keenan, R.J.
Funding support United States, 3items
OrganizationGrant numberCountry
National Institutes of Health/National Institute of General Medical Sciences (NIH/NIGMS)R01 GM086487 United States
National Institutes of Health/National Institute of General Medical Sciences (NIH/NIGMS)U01 GM094588 United States
National Institutes of Health/National Institute of General Medical Sciences (NIH/NIGMS)U54 GM087519 United States
CitationJournal: Science / Year: 2015
Title: Protein targeting. Structure of the Get3 targeting factor in complex with its membrane protein cargo.
Authors: Mateja, A. / Paduch, M. / Chang, H.Y. / Szydlowska, A. / Kossiakoff, A.A. / Hegde, R.S. / Keenan, R.J.
History
DepositionJan 29, 2015Deposition site: RCSB / Processing site: RCSB
Revision 1.0Mar 25, 2015Provider: repository / Type: Initial release
Revision 1.1Sep 20, 2017Group: Author supporting evidence / Database references ...Author supporting evidence / Database references / Derived calculations / Source and taxonomy
Category: citation / entity_src_gen ...citation / entity_src_gen / pdbx_audit_support / pdbx_struct_oper_list
Item: _citation.journal_id_CSD / _entity_src_gen.pdbx_alt_source_flag ..._citation.journal_id_CSD / _entity_src_gen.pdbx_alt_source_flag / _pdbx_audit_support.funding_organization / _pdbx_struct_oper_list.symmetry_operation
Revision 1.2Dec 25, 2019Group: Author supporting evidence / Category: pdbx_audit_support / Item: _pdbx_audit_support.funding_organization
Revision 1.3Sep 27, 2023Group: Data collection / Database references ...Data collection / Database references / Derived calculations / Refinement description
Category: chem_comp_atom / chem_comp_bond ...chem_comp_atom / chem_comp_bond / database_2 / pdbx_initial_refinement_model / pdbx_struct_conn_angle / struct_conn / struct_conn_type / struct_ncs_dom_lim
Item: _database_2.pdbx_DOI / _database_2.pdbx_database_accession ..._database_2.pdbx_DOI / _database_2.pdbx_database_accession / _pdbx_struct_conn_angle.ptnr1_auth_comp_id / _pdbx_struct_conn_angle.ptnr1_auth_seq_id / _pdbx_struct_conn_angle.ptnr1_label_alt_id / _pdbx_struct_conn_angle.ptnr1_label_asym_id / _pdbx_struct_conn_angle.ptnr1_label_atom_id / _pdbx_struct_conn_angle.ptnr1_label_comp_id / _pdbx_struct_conn_angle.ptnr3_auth_comp_id / _pdbx_struct_conn_angle.ptnr3_auth_seq_id / _pdbx_struct_conn_angle.ptnr3_label_alt_id / _pdbx_struct_conn_angle.ptnr3_label_asym_id / _pdbx_struct_conn_angle.ptnr3_label_atom_id / _pdbx_struct_conn_angle.ptnr3_label_comp_id / _pdbx_struct_conn_angle.value / _struct_conn.conn_type_id / _struct_conn.id / _struct_conn.pdbx_dist_value / _struct_conn.pdbx_leaving_atom_flag / _struct_conn.pdbx_ptnr2_label_alt_id / _struct_conn.ptnr1_auth_asym_id / _struct_conn.ptnr1_auth_comp_id / _struct_conn.ptnr1_auth_seq_id / _struct_conn.ptnr1_label_asym_id / _struct_conn.ptnr1_label_atom_id / _struct_conn.ptnr1_label_comp_id / _struct_conn.ptnr1_label_seq_id / _struct_conn.ptnr2_auth_asym_id / _struct_conn.ptnr2_auth_comp_id / _struct_conn.ptnr2_auth_seq_id / _struct_conn.ptnr2_label_asym_id / _struct_conn.ptnr2_label_atom_id / _struct_conn.ptnr2_label_comp_id / _struct_conn.ptnr2_label_seq_id / _struct_conn_type.id / _struct_ncs_dom_lim.beg_auth_comp_id / _struct_ncs_dom_lim.beg_label_asym_id / _struct_ncs_dom_lim.beg_label_comp_id / _struct_ncs_dom_lim.beg_label_seq_id / _struct_ncs_dom_lim.end_auth_comp_id / _struct_ncs_dom_lim.end_label_asym_id / _struct_ncs_dom_lim.end_label_comp_id / _struct_ncs_dom_lim.end_label_seq_id
Revision 2.0Dec 25, 2024Group: Advisory / Atomic model ...Advisory / Atomic model / Data collection / Derived calculations / Structure summary
Category: atom_site / pdbx_entry_details ...atom_site / pdbx_entry_details / pdbx_modification_feature / pdbx_nonpoly_scheme / pdbx_struct_conn_angle / pdbx_validate_close_contact / struct_conn / struct_site / struct_site_gen
Item: _atom_site.B_iso_or_equiv / _atom_site.Cartn_x ..._atom_site.B_iso_or_equiv / _atom_site.Cartn_x / _atom_site.Cartn_y / _atom_site.Cartn_z / _atom_site.auth_asym_id / _atom_site.auth_seq_id / _atom_site.label_asym_id / _pdbx_entry_details.has_protein_modification / _pdbx_nonpoly_scheme.asym_id / _pdbx_nonpoly_scheme.auth_seq_num / _pdbx_nonpoly_scheme.ndb_seq_num / _pdbx_nonpoly_scheme.pdb_seq_num / _pdbx_nonpoly_scheme.pdb_strand_id / _pdbx_struct_conn_angle.ptnr1_auth_asym_id / _pdbx_struct_conn_angle.ptnr1_auth_comp_id / _pdbx_struct_conn_angle.ptnr1_auth_seq_id / _pdbx_struct_conn_angle.ptnr1_label_alt_id / _pdbx_struct_conn_angle.ptnr1_label_asym_id / _pdbx_struct_conn_angle.ptnr1_label_atom_id / _pdbx_struct_conn_angle.ptnr1_label_comp_id / _pdbx_struct_conn_angle.ptnr2_auth_seq_id / _pdbx_struct_conn_angle.ptnr3_auth_asym_id / _pdbx_struct_conn_angle.ptnr3_auth_comp_id / _pdbx_struct_conn_angle.ptnr3_auth_seq_id / _pdbx_struct_conn_angle.ptnr3_label_alt_id / _pdbx_struct_conn_angle.ptnr3_label_asym_id / _pdbx_struct_conn_angle.ptnr3_label_atom_id / _pdbx_struct_conn_angle.ptnr3_label_comp_id / _pdbx_struct_conn_angle.value / _struct_site.details / _struct_site.pdbx_auth_asym_id / _struct_site.pdbx_auth_seq_id / _struct_site_gen.auth_asym_id / _struct_site_gen.auth_seq_id / _struct_site_gen.label_asym_id

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Structure visualization

Structure viewerMolecule:
MolmilJmol/JSmol

Downloads & links

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Assembly

Deposited unit
A: ATPase GET3
B: ATPase GET3
C: Antibody heavy chain
D: Antibody light chain
E: Antibody heavy chain
F: Antibody light chain
G: ATPase GET3
H: ATPase GET3
I: Antibody heavy chain
J: Antibody light chain
K: Antibody heavy chain
L: Antibody light chain
M: ATPase GET3
N: ATPase GET3
O: Antibody heavy chain
P: Antibody light chain
Q: Antibody heavy chain
R: Antibody light chain
S: ATPase GET3
T: ATPase GET3
U: Antibody heavy chain
V: Antibody light chain
W: Antibody heavy chain
X: Antibody light chain
a: Sec22
g: Sec22
m: Sec22
s: Sec22
hetero molecules


Theoretical massNumber of molelcules
Total (without water)722,95556
Polymers715,02428
Non-polymers7,93128
Water7,656425
1
A: ATPase GET3
B: ATPase GET3
C: Antibody heavy chain
D: Antibody light chain
E: Antibody heavy chain
F: Antibody light chain
a: Sec22
hetero molecules


Theoretical massNumber of molelcules
Total (without water)180,73914
Polymers178,7567
Non-polymers1,9837
Water1086
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
2
G: ATPase GET3
H: ATPase GET3
I: Antibody heavy chain
J: Antibody light chain
K: Antibody heavy chain
L: Antibody light chain
g: Sec22
hetero molecules


Theoretical massNumber of molelcules
Total (without water)180,73914
Polymers178,7567
Non-polymers1,9837
Water1086
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
3
M: ATPase GET3
N: ATPase GET3
O: Antibody heavy chain
P: Antibody light chain
Q: Antibody heavy chain
R: Antibody light chain
m: Sec22
hetero molecules


Theoretical massNumber of molelcules
Total (without water)180,73914
Polymers178,7567
Non-polymers1,9837
Water1086
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
4
S: ATPase GET3
T: ATPase GET3
U: Antibody heavy chain
V: Antibody light chain
W: Antibody heavy chain
X: Antibody light chain
s: Sec22
hetero molecules


Theoretical massNumber of molelcules
Total (without water)180,73914
Polymers178,7567
Non-polymers1,9837
Water1086
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Unit cell
Length a, b, c (Å)112.580, 119.450, 147.570
Angle α, β, γ (deg.)71.890, 89.860, 66.610
Int Tables number1
Space group name H-MP1
Noncrystallographic symmetry (NCS)NCS domain:
IDEns-IDDetails
11chain A
21chain B
31chain G
41chain H
51chain M
61chain N
71chain S
81chain T
12chain C
22chain E
32chain I
42chain K
52chain O
62chain Q
72chain U
82chain W
13chain D
23chain F
33chain J
43chain L
53chain P
63chain R
73chain V
83chain X
14chain a
24chain m
34chain s

NCS domain segments:

Component-ID: 1

Dom-IDEns-IDBeg auth comp-IDBeg label comp-IDEnd auth comp-IDEnd label comp-IDSelection detailsAuth asym-IDLabel asym-IDAuth seq-IDLabel seq-ID
11THRTHRLEULEUchain AAA4 - 3504 - 350
21THRTHRASPASPchain BBB4 - 3524 - 352
31THRTHRLEULEUchain GGG4 - 3504 - 350
41VALVALASPASPchain HHH5 - 3525 - 352
51THRTHRLEULEUchain MMM4 - 3504 - 350
61ASPASPASPASPchain NNN2 - 3522 - 352
71THRTHRLEULEUchain SSS4 - 3504 - 350
81ASPASPGLUGLUchain TTT2 - 3512 - 351
12GLUGLUCYSCYSchain CCC4 - 2254 - 225
22GLUGLUCYSCYSchain EEE4 - 2254 - 225
32GLUGLUCYSCYSchain III1 - 2251 - 225
42VALVALCYSCYSchain KKK5 - 2255 - 225
52SERSERCYSCYSchain OOO3 - 2253 - 225
62VALVALCYSCYSchain QQQ5 - 2255 - 225
72GLUGLUCYSCYSchain UUU4 - 2254 - 225
82VALVALCYSCYSchain WWW5 - 2255 - 225
13ASPASPCYSCYSchain DDD2 - 2172 - 217
23ILEILECYSCYSchain FFF3 - 2173 - 217
33ILEILECYSCYSchain JJJ3 - 2173 - 217
43ILEILECYSCYSchain LLL3 - 2173 - 217
53ASPASPCYSCYSchain PPP2 - 2172 - 217
63ASPASPCYSCYSchain RRR2 - 2172 - 217
73ILEILECYSCYSchain VVV3 - 2173 - 217
83ASPASPCYSCYSchain XXX2 - 2172 - 217
14UNKUNKUNKUNKchain aaY1 - 201 - 20
24UNKUNKUNKUNKchain mmAA2 - 201 - 19
34UNKUNKUNKUNKchain ssBA0 - 201 - 21

NCS ensembles :
ID
1
2
3
4

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Components

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Antibody , 2 types, 16 molecules CEIKOQUWDFJLPRVX

#2: Antibody
Antibody heavy chain


Mass: 24560.430 Da / Num. of mol.: 8
Source method: isolated from a genetically manipulated source
Source: (gene. exp.) HOMO SAPIENS, synthetic construct
Description: OBTAINED BY PHAGE DISPLAY FROM A LIBRARY OF HUMAN IGG ANTIBODY FRAGMENT, THE CDRS ARE COMPLETELY SYNTHETIC
Plasmid: RH2.2 / Production host: Escherichia coli (E. coli) / Strain (production host): BL21(DE3)/PRIL
#3: Antibody
Antibody light chain


Mass: 23671.266 Da / Num. of mol.: 8
Source method: isolated from a genetically manipulated source
Source: (gene. exp.) HOMO SAPIENS, synthetic construct
Description: OBTAINED BY PHAGE DISPLAY FROM A LIBRARY OF HUMAN IGG ANTIBODY FRAGMENT, THE CDRS ARE COMPLETELY SYNTHETIC
Plasmid: RH2.2 / Production host: Escherichia coli (E. coli) / Strain (production host): BL21(DE3)/PRIL

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Protein / Protein/peptide , 2 types, 12 molecules ABGHMNSTagms

#1: Protein
ATPase GET3 / Arsenical pump-driving ATPase / Arsenite-stimulated ATPase / Golgi to ER traffic protein 3 / Guided ...Arsenical pump-driving ATPase / Arsenite-stimulated ATPase / Golgi to ER traffic protein 3 / Guided entry of tail-anchored proteins 3


Mass: 39392.605 Da / Num. of mol.: 8 / Mutation: D57N
Source method: isolated from a genetically manipulated source
Source: (gene. exp.) Saccharomyces cerevisiae (ATCC 204508 / S288c) (yeast)
Strain: ATCC 204508 / S288c / Gene: GET3, ARR4, YDL100C, D2371 / Plasmid: pCDF1b / Production host: Escherichia coli (E. coli) / Strain (production host): BL21(DE3)/pRIL
References: UniProt: Q12154, Hydrolases; Acting on acid anhydrides
#4: Protein/peptide
Sec22


Mass: 3507.314 Da / Num. of mol.: 4
Source method: isolated from a genetically manipulated source
Source: (gene. exp.) Saccharomyces cerevisiae (brewer's yeast)
Plasmid: pET28 / Production host: Escherichia coli (E. coli) / Strain (production host): BL21(DE3)/pRIL

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Non-polymers , 5 types, 453 molecules

#5: Chemical
ChemComp-MG / MAGNESIUM ION


Mass: 24.305 Da / Num. of mol.: 8 / Source method: obtained synthetically / Formula: Mg
#6: Chemical
ChemComp-ZN / ZINC ION


Mass: 65.409 Da / Num. of mol.: 4 / Source method: obtained synthetically / Formula: Zn
#7: Chemical
ChemComp-ADP / ADENOSINE-5'-DIPHOSPHATE


Mass: 427.201 Da / Num. of mol.: 8 / Source method: obtained synthetically / Formula: C10H15N5O10P2 / Comment: ADP, energy-carrying molecule*YM
#8: Chemical
ChemComp-ATP / ADENOSINE-5'-TRIPHOSPHATE


Mass: 507.181 Da / Num. of mol.: 8 / Source method: isolated from a natural source / Formula: C10H16N5O13P3 / Comment: ATP, energy-carrying molecule*YM
#9: Water ChemComp-HOH / water


Mass: 18.015 Da / Num. of mol.: 425 / Source method: isolated from a natural source / Formula: H2O

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Details

Has protein modificationY
Sequence detailsThe sequence of the bound peptide is:MGSHHHHHHSKINFDLLISQYAPIVIVAFFFVFLFWWIFLK However, due to ...The sequence of the bound peptide is:MGSHHHHHHSKINFDLLISQYAPIVIVAFFFVFLFWWIFLK However, due to relatively poor local density, this chain was modeled as a poly-alanine helix

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Experimental details

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Experiment

ExperimentMethod: X-RAY DIFFRACTION / Number of used crystals: 1

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Sample preparation

CrystalDensity Matthews: 2.4 Å3/Da / Density % sol: 48.7 %
Crystal growTemperature: 298 K / Method: vapor diffusion, hanging drop / Details: 13% PEG 3350, 25 mM succinic acid pH 7.0

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Data collection

DiffractionMean temperature: 100 K
Diffraction sourceSource: SYNCHROTRON / Site: APS / Beamline: 24-ID-C / Wavelength: 0.9795 Å
DetectorType: DECTRIS PILATUS 6M-F / Detector: PIXEL / Date: Mar 10, 2014
RadiationProtocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelengthWavelength: 0.9795 Å / Relative weight: 1
ReflectionResolution: 2.75→39.723 Å / Num. obs: 157053 / % possible obs: 91 % / Redundancy: 1.7 % / Net I/σ(I): 8.2
Reflection shellResolution: 2.75→2.85 Å / Redundancy: 1.7 % / Mean I/σ(I) obs: 1.4 / % possible all: 89

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Processing

Software
NameClassification
PHENIXrefinement
xia2data reduction
Cootmodel building
PHASERphasing
RefinementMethod to determine structure: MOLECULAR REPLACEMENT
Starting model: 2woj, 3pgf

2woj

3pgf


Resolution: 2.75→39.723 Å / SU ML: 0.42 / Cross valid method: FREE R-VALUE / σ(F): 1.97 / Phase error: 28.91 / Stereochemistry target values: ML
RfactorNum. reflection% reflection
Rfree0.2472 7818 5 %
Rwork0.1956 148484 -
obs0.1983 156302 90.62 %
Solvent computationShrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å / Solvent model: FLAT BULK SOLVENT MODEL
Displacement parametersBiso max: 278.83 Å2 / Biso mean: 75.163 Å2 / Biso min: 17.19 Å2
Refinement stepCycle: final / Resolution: 2.75→39.723 Å
ProteinNucleic acidLigandSolventTotal
Num. atoms45612 0 660 425 46697
Biso mean--50.44 51.43 -
Num. residues----5938
Refine LS restraints
Refine-IDTypeDev idealNumber
X-RAY DIFFRACTIONf_bond_d0.00547135
X-RAY DIFFRACTIONf_angle_d0.80663950
X-RAY DIFFRACTIONf_chiral_restr0.0317267
X-RAY DIFFRACTIONf_plane_restr0.0048057
X-RAY DIFFRACTIONf_dihedral_angle_d12.30717009
Refine LS restraints NCS
Ens-IDDom-IDAuth asym-IDNumberRefine-IDRmsType
11A11615X-RAY DIFFRACTION10.585TORSIONAL
12B11615X-RAY DIFFRACTION10.585TORSIONAL
13G11615X-RAY DIFFRACTION10.585TORSIONAL
14H11615X-RAY DIFFRACTION10.585TORSIONAL
15M11615X-RAY DIFFRACTION10.585TORSIONAL
16N11615X-RAY DIFFRACTION10.585TORSIONAL
17S11615X-RAY DIFFRACTION10.585TORSIONAL
18T11615X-RAY DIFFRACTION10.585TORSIONAL
21C7964X-RAY DIFFRACTION10.585TORSIONAL
22E7964X-RAY DIFFRACTION10.585TORSIONAL
23I7964X-RAY DIFFRACTION10.585TORSIONAL
24K7964X-RAY DIFFRACTION10.585TORSIONAL
25O7964X-RAY DIFFRACTION10.585TORSIONAL
26Q7964X-RAY DIFFRACTION10.585TORSIONAL
27U7964X-RAY DIFFRACTION10.585TORSIONAL
28W7964X-RAY DIFFRACTION10.585TORSIONAL
31D8179X-RAY DIFFRACTION10.585TORSIONAL
32F8179X-RAY DIFFRACTION10.585TORSIONAL
33J8179X-RAY DIFFRACTION10.585TORSIONAL
34L8179X-RAY DIFFRACTION10.585TORSIONAL
35P8179X-RAY DIFFRACTION10.585TORSIONAL
36R8179X-RAY DIFFRACTION10.585TORSIONAL
37V8179X-RAY DIFFRACTION10.585TORSIONAL
38X8179X-RAY DIFFRACTION10.585TORSIONAL
41a162X-RAY DIFFRACTION10.585TORSIONAL
42m162X-RAY DIFFRACTION10.585TORSIONAL
43s162X-RAY DIFFRACTION10.585TORSIONAL
LS refinement shell

Refine-ID: X-RAY DIFFRACTION / Total num. of bins used: 30

Resolution (Å)Rfactor RfreeNum. reflection RfreeRfactor RworkNum. reflection RworkNum. reflection all% reflection obs (%)
2.75-2.78190.3742480.2994488473682
2.7819-2.81460.37012520.29825042529493
2.8146-2.84890.33272620.2945107536993
2.8489-2.8850.36872390.28575072531193
2.885-2.92290.34442760.28065052532893
2.9229-2.9630.33452470.27645109535693
2.963-3.00530.31242610.28115053531493
3.0053-3.05010.35012420.28485138538093
3.0501-3.09780.34292710.26984961523292
3.0978-3.14850.3462670.26374943521091
3.1485-3.20280.32032610.25444795505688
3.2028-3.2610.30982400.24764995523592
3.261-3.32370.28172650.23325129539493
3.3237-3.39150.29642910.23245047533893
3.3915-3.46520.272670.22395051531893
3.4652-3.54580.26482650.22015131539693
3.5458-3.63440.26042680.20895024529292
3.6344-3.73260.28522800.20214971525191
3.7326-3.84230.26422370.19294895513290
3.8423-3.96620.22742640.18064704496886
3.9662-4.10790.22112940.17235058535293
4.1079-4.27210.2182500.15815064531492
4.2721-4.46630.20292850.14334957524291
4.4663-4.70150.19322670.14354934520190
4.7015-4.99550.1872330.1394905513889
4.9955-5.38030.1952880.14834729501787
5.3803-5.92020.22442660.1644949521591
5.9202-6.77320.24462380.1744878511689
6.7732-8.51960.19172410.16784718495986
8.5196-39.72660.18532530.17024585483884
Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

IDL11 (°2)L12 (°2)L13 (°2)L22 (°2)L23 (°2)L33 (°2)S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T11 (Å2)T12 (Å2)T13 (Å2)T22 (Å2)T23 (Å2)T33 (Å2)Origin x (Å)Origin y (Å)Origin z (Å)
13.11221.22551.04613.1969-0.75823.54890.1851-1.05640.58020.5381-0.4739-0.4773-0.08750.44970.26730.4562-0.1786-0.10560.7927-0.07960.4104100.5667-241.9558-122.0167
28.3086-0.1512-2.52386.06-0.73990.92530.8077-0.3401-0.20850.463-0.4777-1.05040.05660.8899-0.1230.8843-0.1644-0.10040.94830.0420.772110.1883-266.0229-127.1196
32.5583-0.3343-1.92537.95252.39212.31420.0767-1.1793-0.31230.9608-0.1479-0.15360.6610.1910.05380.5939-0.09-0.04070.87810.06260.36699.097-254.6398-119.0569
41.7825-0.8793-0.02226.0921-0.78573.5663-0.4811-1.0175-0.73761.99860.58920.90391.37220.05480.02411.4135-0.03850.06831.16950.16580.440694.6999-265.2093-110.6634
56.67451.63421.77754.5573-2.23344.92470.0512-0.32620.56910.29310.0110.4943-0.1866-0.0976-0.09540.2607-0.00680.06650.4338-0.1390.426883.6089-242.8657-126.7857
64.9925-0.959-0.25410.4645-0.34941.57460.2263-0.23311.49550.098-0.08410.0996-0.72980.2017-0.14220.5627-0.09560.06920.392-0.0770.875886.8279-231.586-131.6973
75.55250.0858-0.31043.33010.60013.6803-0.1255-0.0174-0.31360.0941-0.1970.24060.49-0.31080.29650.3436-0.04210.00690.3406-0.07390.290882.9859-260.997-147.2406
87.6654-0.453.25053.7543-1.22298.0954-0.0405-0.1211-0.99980.4160.23340.28931.18660.62020.09380.62030.04440.00540.34640.02040.519989.3389-268.5661-137.9372
93.93360.1041-0.63270.96721.13852.4864-0.1535-0.1668-0.38850.14630.1585-0.20750.54790.2965-0.09390.38680.0628-0.01470.47930.05310.377499.2129-261.9204-144.8447
105.6822.8825-1.42343.1724-0.23641.4310.19770.6020.9159-0.22660.00630.2811-0.4909-0.1461-0.17090.48140.05520.04670.49780.1790.446788.5933-241.566-153.3145
118.152.5792-2.78781.8403-0.6122.8366-0.0699-0.2694-0.55270.0944-0.11730.18060.22910.16330.24120.35810.09050.0620.27890.00140.389756.2006-257.9327-127.142
124.11370.10420.57126.1144-0.6153.9394-0.1312-0.4519-0.1722-0.0662-0.00470.25440.3177-0.9270.20720.4096-0.05790.0640.55350.0060.303519.9083-256.376-117.6819
137.0096-2.2288-0.45447.5459-1.2124.9597-0.2706-1.54930.10161.11180.33581.1473-0.38150.03610.1310.4149-0.13790.12480.5987-0.30590.63550.2631-238.1526-110.5739
147.4977-1.6509-1.42222.96180.43785.86650.3602-0.53411.10390.0733-0.1499-0.0623-0.4490.2164-0.13060.4109-0.08980.12360.3866-0.12860.530154.8329-237.1953-118.6567
159.6015-2.085-4.12951.23290.35393.1346-0.0892-0.76670.49390.5230.1682-0.27220.16010.2061-0.15410.4439-0.07020.02040.6056-0.2460.481750.4199-242.4623-113.4473
162.5757-1.2033-0.96043.69-1.01142.9444-0.08630.00630.01080.22640.1448-0.05660.1397-0.02390.00730.3688-0.06330.00460.4350.01810.339124.175-253.6101-104.8544
172.87980.5025-3.01892.1935-3.56989.5755-0.3179-0.8409-0.16730.3151-0.4945-0.39090.35631.66890.54520.38830.0494-0.02070.9480.11750.546330.4629-257.1557-99.3454
183.59960.98-1.07055.81031.97532.93750.2458-0.6042-0.12620.4045-0.42760.00870.07950.02250.14630.31580.03430.01910.5515-0.02550.332525.9756-253.178-104.4479
198.51316.4596-6.1155.7064-6.18798.2618-0.39550.5574-0.14320.61380.84010.4352-0.6291-0.5823-0.37030.58760.03130.04150.75540.00790.559519.1373-250.0611-97.2954
202.70370.1234-0.35371.30571.02611.45930.0733-1.51550.62660.07730.1654-0.49340.09240.40360.06280.4270.02770.08610.51470.19390.3566133.8944-241.8167-139.2845
213.2571-0.4125-0.07092.2216-0.23761.3864-0.2179-0.3105-0.23790.09220.04370.0870.1665-0.0056-0.00740.3773-0.01150.00070.46210.19660.4024124.9082-244.4212-143.9109
222.1202-1.08630.69974.50340.00332.7685-0.0347-0.5817-0.4673-0.183-0.52950.99350.3795-0.40580.0490.51250.01350.09630.28480.58490.3638122.9113-253.0463-140.5379
234.9647-0.5196-0.47520.8942-0.92561.2456-0.0975-0.4209-0.07610.22170.05580.11670.04510.22760.01680.4394-0.021-0.01030.41510.16280.3674130.5282-244.5545-143.266
247.6558-2.20784.59252.7149-1.33422.73840.2581.78550.44960.253-0.05790.4913-0.24610.4344-0.21560.525-0.0945-0.04290.64650.02030.5292167.372-236.5421-163.6304
251.35260.64760.432.1428-2.19454.18320.4389-0.12340.60150.1091-0.13290.3279-0.7741-0.1471-0.35990.47430.08780.02890.24920.12550.6042157.3638-235.7513-151.7566
264.2148-0.13880.13741.13661.41463.96970.03140.18980.50720.40850.1444-0.5176-0.92110.0589-0.18480.3859-0.0165-0.03870.24420.11920.5536159.072-234.6462-158.5072
279.39115.52011.87547.0926-3.55816.06530.2981-1.0461.10060.7292-0.1336-0.1815-1.16030.97660.06580.50760.0056-0.06420.4068-0.02830.4654163.6147-232.7315-149.5101
283.41672.9822-2.98294.4723-5.81418.15720.11751.1905-0.6352-0.3615-0.6405-0.9903-0.0274-0.16990.64410.41370.12710.02830.55390.1140.4463129.6721-244.815-169.7883
294.01010.5185-0.27140.5966-0.65465.54750.01930.11820.13130.0701-0.1162-0.1232-0.12360.16840.08890.27230.0643-0.00140.35430.15590.3973122.8949-241.0925-163.982
306.6711.9222-3.66860.3871-0.66666.4009-0.37630.7345-0.6803-0.30720.0782-0.18070.7917-0.56150.24940.38090.18440.03040.39290.25470.5214130.4518-245.7027-163.5814
316.5669-1.01890.73773.055-2.10924.5277-0.21490.1325-0.2061-0.18540.31930.00330.192-0.2177-0.09490.3848-0.0442-0.02780.2190.0570.4128158.8759-245.8188-163.2837
322.5052-3.54723.5075.9838-4.20438.49160.11880.07260.0488-0.2824-0.3655-0.97030.39110.05910.58010.4134-0.01620.13580.53810.04760.6843166.1603-248.9782-169.7179
333.2917-0.0604-0.03245.2208-2.12235.2577-0.2501-0.60850.71450.5582-0.33490.2667-0.2788-0.24750.36520.2548-0.0715-0.01540.4164-0.21070.45957.5965-161.1964-47.3507
346.54811.3460.20454.70850.36043.4683-0.1205-0.32480.1634-0.05580.0784-0.38140.4960.51180.03540.37730.0391-0.05020.46190.01450.325972.9145-165.8131-53.4227
357.59241.56541.84247.15363.32936.9916-0.0573-0.4254-0.76240.6664-0.0643-0.30431.10010.53750.15680.5410.0655-0.04110.51160.0640.385667.7872-177.6437-51.6398
365.9253-0.21090.62121.7946-0.44343.45090.0353-0.9169-0.66160.208-0.10230.12831.06390.1212-0.14750.64710.04080.07590.45510.09270.280456.0496-177.684-48.2855
375.73623.8395-2.78366.5167-0.90782.47530.1993-0.10921.3586-0.14850.59711.3326-0.6125-0.1439-0.55890.41380.0305-0.05080.3715-0.0130.70651.0156-153.6676-60.3103
385.4295-0.41971.18922.4319-0.16282.23350.21480.02621.2532-0.0175-0.05420.1012-0.63330.0611-0.13440.40090.02610.02980.2764-0.03970.629653.6342-151.4995-60.0378
394.5910.26540.65273.8917-0.11781.78030.00960.6504-0.4534-0.0253-0.03980.14770.3975-0.31880.1620.3348-0.02-0.00480.5293-0.1450.261550.1529-179.4167-78.0306
402.32490.59750.59882.62760.21954.7596-0.09540.1658-1.2098-0.2263-0.26060.76740.5805-1.01620.81030.65310.093-0.00410.5995-0.14190.88655.0424-191.3388-66.5692
415.04430.17610.04795.09630.46513.4439-0.30610.2559-1.3305-0.0228-0.1078-0.86931.29970.32410.21840.79380.08850.20610.5628-0.10250.659864.5382-192.6983-72.5731
423.99191.6081-1.12463.47261.09311.9673-0.03860.98820.7917-0.42010.1552-0.2083-0.24590.0252-0.0330.4052-0.0293-0.01950.70030.22050.309259.8255-162.7257-80.7088
435.7591-0.3492-1.71188.2958-4.01588.0078-0.48960.8714-0.6721-0.90270.1916-0.18510.5025-0.15010.29240.298-0.0439-0.05010.3604-0.1880.322620.0089-177.7924-64.6704
445.57091.0875-1.21393.2503-0.31261.5028-0.17710.1413-0.5959-0.1174-0.01350.03520.17220.17530.18890.28570.05860.01130.1756-0.04070.258524.1958-177.9529-57.609
457.2042-1.10190.27966.0496-0.00094.0093-0.2863-0.0247-0.5568-0.09660.2790.20120.2703-1.01230.03520.3121-0.0464-0.00560.41960.06770.3649-12.7802-178.3043-49.1374
466.5432-5.1008-1.08638.4262-1.51075.44540.1895-1.13510.51250.9141-0.13640.5672-0.72130.76470.18430.360.0212-0.01030.1884-0.12870.656616.5377-160.1146-39.5078
473.75230.2119-1.9323.37890.22233.3203-0.0474-0.12620.9083-0.00430.03420.2103-0.42840.2522-0.04010.3888-0.0169-0.04690.1393-0.09110.447621.9413-159.0571-47.3608
489.17642.2633-1.4236.9801-1.84482.898-0.0208-1.3367-0.620.93560.0433-0.84650.13660.5705-0.08060.33010.0202-0.04580.4862-0.0580.375630.9163-170.3654-46.5802
496.4125-1.601-1.4870.46590.21560.4545-0.3794-1.00320.6890.41710.3822-0.26910.01820.3147-0.04720.47390.1389-0.06330.2698-0.0250.56682.3129-159.1912-38.4081
504.76011.7278-0.71118.476-2.4574.752-0.2681-0.4958-0.6191-0.2310.2861-0.02390.19-0.78290.00320.25290.07390.01030.47730.0520.3837-8.2269-178.0806-36.1146
510.76181.56220.41925.4807-3.25866.64290.428-0.74060.18690.2090.15290.47580.16190.1756-0.44420.3310.11720.00920.62050.10670.5402-1.5627-182.4415-31.7232
524.77022.0007-0.14046.5544-1.59733.05210.0067-0.4666-0.2563-0.06470.1640.34920.1921-0.4605-0.16380.2060.09390.02470.42660.02920.3354-6.3347-177.5653-35.5753
536.68773.5494-1.47313.1635-2.67925.08020.2006-0.56110.06820.79750.10891.76-0.2851-1.1729-0.06890.41220.20.01380.98890.15240.7676-12.4447-176.0174-27.572
547.3366-1.2487-1.86012.08170.71931.1573-0.2858-0.3361-0.16680.12190.09080.12890.15320.32510.15210.36260.02210.00830.60070.18520.346893.4527-165.0074-71.0821
554.8287-0.7474-1.04510.8395-0.93472.6481-0.1954-0.9395-0.20640.05530.2030.06250.21710.2682-0.00870.36250.0087-0.01050.69110.17770.412497.6938-162.6812-72.3051
566.0868-3.01222.38165.1893-0.79410.9705-0.63060.88430.4196-0.37680.2217-0.91950.1168-0.87010.05760.3732-0.1007-0.00110.79810.15760.6904131.5211-155.5917-86.5949
574.07662.0199-0.05972.569-1.75767.5202-0.4997-1.04250.8705-0.27340.26820.0376-1.5828-0.6766-0.62320.46180.21960.18020.6193-0.06610.7495122.2959-150.7017-78.471
584.6891.39071.94842.5708-1.3376.6602-0.1915-0.15560.88340.15430.472-0.3828-0.46-0.7064-0.47360.33760.08320.08870.58880.10020.6803121.2649-156.0113-84.5413
593.1577-1.236-0.33471.44950.82678.3726-0.30410.16682.2415-0.11360.2102-0.463-1.66080.86430.23660.6746-0.0728-0.12280.7770.41541.3682130.8049-148.1675-89.6878
606.96615.6546-4.56165.1461-3.77173.69830.49330.04830.61520.41840.5252-0.1361-0.1680.7462-1.22460.82660.03760.01311.1499-0.03011.0018131.0885-150.6538-78.2841
614.46822.5507-0.58597.7333-2.82075.6305-0.93161.33680.0371-0.60151.0073-0.3455-0.0593-0.2453-0.15420.4201-0.02740.01910.94080.13620.612896.8223-160.7106-98.5579
625.70330.962-1.11690.6452-0.93793.6603-0.19451.15440.6794-0.0594-0.02360.03740.1440.08350.2110.3959-0.0078-0.02890.73760.22390.414389.0758-157.9951-90.4183
633.1829-1.3674-0.73020.86130.27592.7058-0.20751.38830.6088-0.1718-0.0653-0.0466-0.0139-0.04560.2440.3795-0.089-0.07381.21280.37620.519391.4035-156.8805-95.4137
646.06251.0792-0.29718.5416-1.53135.3671-0.28120.861-1.6428-0.84080.22740.38280.7293-0.2130.06420.5157-0.0806-0.0550.94330.04350.405587.2668-169.4934-84.8398
650.0026-0.0276-0.01220.74150.30180.0892-0.79731.03050.3677-0.65460.0386-0.5194-0.03120.41380.58670.5525-0.09620.06721.7410.48630.663109.5118-153.9113-101.6662
664.1788-0.6102-2.99036.1799-0.47012.7359-0.2903-0.0283-0.1406-0.67330.3525-0.2187-0.0458-0.2395-0.07130.4137-0.06890.06910.75080.03330.4476127.7192-162.1369-92.9022
675.7715-0.8343-1.03261.810.50820.35710.36681.1340.5509-1.14790.143-1.33040.0868-0.6048-0.44420.71-0.18850.23640.8896-0.0350.6069125.5218-171.0497-92.845
685.045-1.73850.5542.9248-1.45042.0394-0.35220.04320.23790.29890.3510.1505-0.14240.23770.07440.5149-0.02360.16940.95960.04310.5315122.6571-159.5772-91.5244
697.978-4.66523.63737.0648-4.012.853-0.27860.37370.0542-0.3559-0.2845-0.8396-0.09650.32920.66850.5646-0.04590.1411.27530.02940.7037132.7389-166.0349-99.214
701.8134-0.44560.76715.4638-1.01863.1048-0.005-0.10160.44560.2569-0.1346-0.2635-0.25920.49240.1220.4187-0.1083-0.01070.3287-0.07970.382993.3915-166.2746-156.7269
716.0977-1.84050.84113.3728-1.03053.12550.0625-0.9087-0.01761.21220.0439-0.24850.24350.5902-0.12410.8208-0.0061-0.09370.5874-0.09740.413993.0181-176.4565-143.1601
723.00880.42980.99721.2513-0.01283.59090.02610.21770.2709-0.05290.02790.37850.0076-0.31980.01610.37420.05740.02640.2799-0.06890.562876.3491-168.1831-168.2592
733.89290.04250.08572.9580.50453.03340.02190.2655-0.2998-0.2273-0.00860.18120.2242-0.21470.06220.40240.0481-0.10360.2396-0.1020.368689.1745-194.7219-176.8396
744.86131.53972.01164.51532.87463.2608-0.0769-1.4007-0.13171.2493-0.87771.25580.9279-1.32670.06860.6613-0.03490.01190.4966-0.08980.551686.3611-196.0766-156.909
752.9733-0.0536-0.87963.4895-0.49533.6838-0.0895-0.3984-0.2840.32570.0191-0.20450.37680.49880.10810.45360.0664-0.05370.3678-0.1130.3771101.7218-193.7471-164.7637
769.9803-4.88510.44147.7189-2.65461.98360.4492.3754-0.0172-0.2317-0.82180.35650.78350.0011-0.40020.78770.0844-0.06480.3108-0.16250.270991.383-177.7403-184.3694
772.34430.36910.24144.8317-0.93190.48080.09770.83050.0011-0.57080.10490.5201-0.10190.0137-0.15780.42650.0587-0.1050.5253-0.04720.324787.2327-179.3806-186.6382
785.42860.06521.36463.3164-2.71054.16180.71520.9216-1.0412-0.7365-0.37120.09711.29770.23770.24530.6123-0.1166-0.14660.1358-0.20530.740754.7505-203.7764-162.2409
792.64020.3485-1.20894.0437-1.42854.34190.0716-0.1477-0.32070.19670.02190.22920.32810.2601-0.08690.4317-0.0518-0.04180.1999-0.10710.425861.2003-195.2318-158.3782
804.39871.9731-1.02151.6865-0.21522.0060.0791-0.2940.01950.23050.00510.04030.15480.1392-0.14230.5156-0.0158-0.04340.2296-0.0780.480755.2764-198.9489-159.0368
812.74843.378-0.35524.299-1.35415.91030.0422-0.01680.29731.3166-0.2621.4030.6822-1.9646-0.07770.5566-0.21020.14730.9208-0.23070.742121.2893-210.2116-154.1254
824.43651.81830.24995.1265-0.86624.9690.47190.6904-0.035-0.1235-0.48710.32250.8992-0.21750.13540.44420.1036-0.03490.5883-0.04690.406130.8597-210.511-161.8113
834.69432.01030.91597.0939-1.41734.89280.13420.2434-0.05160.9673-0.23591.6421-0.0796-1.3936-0.40640.4523-0.09930.08991.02-0.16910.741225.4044-205.4555-156.7496
849.1767-0.5784-1.70679.3627-0.5947.02410.38451.91370.33610.2749-0.45460.9436-0.0306-0.34770.05630.7566-0.10420.01220.5781-0.08150.552423.1889-213.8415-163.2152
857.03670.16770.62439.387-0.34055.4755-0.13040.5896-0.42631.0410.00472.0026-0.159-1.34810.35430.9606-0.13930.09480.6916-0.16971.034719.6867-217.5483-158.4377
865.15090.54951.02326.19010.29516.71090.7909-0.44691.06320.3139-0.66320.98320.0202-0.0439-0.04570.54530.00270.21910.5914-0.04720.875540.9655-178.3355-153.1909
875.3094-0.797-2.2424.30920.39322.77020.282-0.08050.80650.1957-0.0480.6269-0.4145-0.0345-0.22070.47010.00160.08630.2737-0.0670.806348.6511-179.0636-159.2158
880.0529-0.00610.1694-0.0146-0.03170.4319-0.25780.63050.63720.0391-0.13011.96740.1221-1.12410.1040.3751-0.02790.20591.0605-0.24261.68325.9752-184.1229-156.2756
894.49130.24320.07434.1693-0.04552.96560.1322-0.66620.67651.8118-0.51071.51010.4302-0.91380.29530.9583-0.22990.44530.9267-0.27190.976120.8387-203.304-146.897
902.1774-0.672-0.27632.4464-3.19635.02040.0174-1.00470.69331.88150.16860.73810.5304-0.867-0.48241.5569-0.36080.4581.4653-0.34940.892425.1844-202.1657-138.413
912.3999-2.37120.62232.8781-1.20380.79450.7821.73431.17410.0724-1.61060.4105-0.0145-0.70820.59250.65150.02790.01151.1617-0.00080.893525.6376-191.4963-160.024
924.3645-0.29580.01571.08812.08974.12150.8002-1.0573-0.26112.482-0.43891.9630.5623-0.2399-0.66921.4969-0.32790.41081.118-0.03740.876422.9613-211.2623-139.732
933.7593-1.28630.55375.8298-4.59585.2138-0.2073-1.1975-0.03240.17070.94450.3807-0.6282-0.9488-0.69721.2995-0.20290.7441.3811-0.25361.492114.2572-200.6466-141.1522
947.32560.44730.78033.9001-0.19874.81660.0766-0.82780.76520.3863-0.13680.1157-0.2017-0.42660.01310.477-0.02250.06190.432-0.15090.3114120.8714-162.4846-170.9418
956.98651.8347-0.76824.6197-0.60536.50570.0435-0.2508-0.8409-0.1879-0.0036-0.01040.5946-0.2552-0.0640.46460.0164-0.08970.31890.03150.3373121.5437-172.4136-171.6676
966.97820.74580.61121.1697-0.04270.3724-0.023-0.48910.1166-0.05670.1496-0.1564-0.09710.0341-0.10520.47460.03330.04650.4486-0.12130.3487128.0664-163.8205-173.1782
978.9772-1.3034.51044.25240.70963.2890.17863.85421.1078-1.5384-0.0576-0.9789-0.02610.9211-0.46541.14340.06440.52121.35950.04551.3659164.8707-153.1827-196.3216
982.40860.21510.17644.54260.71715.97870.0290.01510.62870.45760.30170.4441-0.7693-0.6295-0.22180.48070.10090.18180.3832-0.04260.738150.5108-154.4835-180.9113
992.84441.4321.22776.28092.18743.72730.10140.2411.1881-0.26190.3251-0.8652-1.38330.7307-0.2930.86970.080.12170.5229-0.00381.1955157.977-148.7562-188.8296
1002.87591.6641.28263.8245-3.69677.2955-0.1462-0.34550.88790.61590.494-1.0938-1.88660.1258-0.4831.0185-0.11570.23340.5311-0.23981.1539156.7865-148.1193-177.2738
1017.67460.02280.51922.751-3.73498.9902-0.24011.6755-1.10640.0907-0.6271-0.52520.43660.77510.33020.7247-0.12320.14240.8387-0.30280.5012128.8023-172.338-196.6061
1027.18451.226-1.06341.6576-0.43343.5537-0.06181.0397-0.1137-0.46270.06020.0086-0.1672-0.0167-0.03430.51710.0015-0.02770.66760.00450.2745119.3983-168.3665-192.119
1035.75911.8531-0.99660.715-0.87562.325-0.24471.4064-0.52-0.51610.3662-0.48660.2126-0.51070.01490.6352-0.011-0.02950.8389-0.220.3716118.5003-173.9508-198.2961
1047.95381.0145-0.62282.91710.26682.95140.19431.19720.6084-0.67710.17470.445-0.56190.6459-0.170.47480.0426-0.01280.6146-0.00650.3954125.4805-163.8056-195.7626
1054.2239-0.281-0.02341.53910.5363.34360.13860.5194-0.251-0.3685-0.25290.13350.13230.20770.16170.5582-0.078-0.00870.6042-0.05410.405128.851-170.5643-191.3441
1067.0537-0.70751.89976.1165-0.06097.8442-0.08750.2508-0.2052-0.19820.0035-1.0512-0.1951.89330.09020.4255-0.11550.15420.5114-0.10120.7328164.1056-159.043-182.7287
1077.7027-1.34616.61062.0864-0.6446.12280.3016-0.0897-0.6281-0.45870.0227-0.12610.7536-0.3569-0.25570.6546-0.18280.24380.6084-0.05340.5174154.527-165.7954-192.3921
1082.86330.56071.54920.2985-0.29412.8305-0.45860.1044-0.934-0.51880.358-0.72831.3187-0.07130.3090.9409-0.02290.35810.559-0.25031.0831157.9958-172.0651-186.469
1094.36680.71941.13751.4017-1.12095.1811-0.05760.5823-0.3175-0.0459-0.0362-0.06630.0094-0.34310.11420.47940.01960.12740.5459-0.14920.5316152.4213-161.8677-188.6646
1105.9159-1.53050.7951.7989-1.38425.6186-0.47210.50680.6804-0.0167-0.4039-0.65770.72330.68620.43550.73070.14160.03350.6247-0.13730.8258166.6828-169.7202-188.3368
1114.6397-3.25274.12362.2355-2.89093.74740.01431.1216-0.05330.2049-0.1606-0.00660.30990.46260.04380.5923-0.00690.18351.0144-0.19220.9399163.9772-165.3267-196.1878
1121.74110.8434-0.14894.9048-1.60483.6205-0.37260.02170.18750.2760.03840.5753-0.5830.40760.31910.5188-0.16210.08420.5427-0.11160.749115.8106-189.4699-85.8061
1133.871-0.21151.4617.1041-2.49473.44670.3315-0.67950.40610.0226-0.5269-1.1492-0.13950.45050.20070.5115-0.24030.0360.92-0.06140.6333130.8219-191.5133-90.8528
1144.6417-3.85310.61237.4967-1.62722.42980.17850.72840.35990.2297-0.6878-1.16910.26980.95190.39970.8051-0.19720.0020.9648-0.11130.6226137.2581-203.9224-83.8925
1152.8196-0.7334-0.02585.0436-1.15134.2301-0.1499-0.2582-0.18320.66320.28420.1862-0.26520.441-0.05060.7414-0.096-0.00090.8391-0.26450.5168124.5083-203.4032-74.2266
1163.9521-0.59451.34110.8035-2.08675.73020.43990.07070.0210.19210.18280.20240.6339-0.5958-0.53080.6466-0.20020.06250.6334-0.17510.7188109.0801-203.8549-87.8926
1174.72910.65690.18753.5517-0.07189.2127-0.12030.32680.7760.01960.1441.1466-0.7761-0.81370.1190.4762-0.0111-0.06220.5907-0.06790.9731103.6231-197.6287-101.4746
1184.42182.4010.50256.5719-0.39727.31880.32630.08831.18950.028-0.09631.1661-1.1809-0.0415-0.21380.59250.04010.01470.5307-0.04780.7747111.091-186.7567-99.145
1194.32821.16970.51363.6472-0.38552.7469-0.0543-0.0191-0.3725-0.02260.07340.15140.0958-0.13060.03240.4434-0.1202-0.02760.543-0.17310.4443119.0513-222.1173-104.5301
1204.29620.32710.24778.38250.93974.4812-0.6372-1.1885-0.44660.34150.66680.5512-0.61930.7873-0.02190.51190.0545-0.04160.7151-0.04580.4238124.9994-226.5672-88.4254
1214.5373-1.38942.31217.33340.47912.1296-0.3806-0.5418-0.19661.01180.1985-0.33580.06140.15020.15790.6936-0.12290.13140.8134-0.15410.4541133.2443-223.0484-91.2671
1226.1167-1.87041.66254.57560.3893.7675-0.3932-1.34610.25280.5765-0.4628-0.89361.2404-0.24970.61870.7067-0.0298-0.00440.7533-0.18620.6055138.2885-230.6353-90.7708
1233.5352-1.3387-0.6654.5142-0.11380.44360.13480.53690.2173-0.1687-0.0633-0.252-0.02620.0337-0.06250.6063-0.11750.0050.6002-0.09930.291128.9792-207.9704-108.1497
1240.78380.4281-0.56123.7594-0.28321.2295-0.29690.8610.3598-0.45960.29760.4872-0.4238-0.4624-0.03310.6401-0.0725-0.11330.96320.00690.4383118.1316-205.6921-116.8101
1257.83663.5435-3.31594.5633-1.5593.7126-0.0645-0.0719-0.43690.0092-0.18820.3380.14780.39940.1980.3628-0.02260.00790.7754-0.07580.567988.6968-224.0374-90.2868
1268.141.5754-0.0466.4428-0.62185.44130.0551-1.0141-1.07320.4237-0.359-0.14320.02621.04350.32420.5191-0.0180.09220.8490.02360.69292.6596-225.4391-85.1288
1278.39762.3583-2.51785.0619-3.16924.8616-1.02961.45340.9135-0.62471.09840.2237-0.00970.1244-0.12890.4319-0.1231-0.05430.7-0.18050.91189.5414-212.9807-94.6968
1287.9154.5528-2.00137.0236-2.70393.7266-0.4710.5736-2.57990.28980.1121-0.45371.1103-1.0727-0.05270.7725-0.2256-0.00970.7822-0.09931.618876.0323-238.6071-82.0088
1293.18591.16461.26890.67731.12972.0921-0.27490.9468-2.0124-0.5978-0.50550.18120.40860.5940.72150.9230.05280.00552.1056-0.14421.852158.4877-238.068-85.9833
1300.33690.2681-0.16138.3172.78191.1193-1.10181.1167-0.3709-0.48830.03731.7748-0.12420.67740.65291.08110.0147-0.0811.9520.28882.142154.4043-232.3333-96.0775
1315.4245-0.2305-3.56544.75882.75093.8111-0.3257-0.2497-0.99541.15350.60371.26451.30780.036-0.03121.1490.15960.3951.3630.21141.939866.2094-234.2078-78.4944
1320.5476-1.483-1.26683.99633.58043.1526-0.25740.0503-1.4948-0.8074-0.12482.90310.3923-2.30460.52211.1445-0.0795-0.24082.2617-0.25342.699946.1205-235.2878-92.132
1331.0008-0.81840.84050.7396-0.38161.82861.84350.5070.20510.13990.29340.62761.20250.8437-1.50931.09850.00430.19812.5038-0.10112.583256.7433-244.0846-89.6967
1342.1937-0.7436-1.08790.26830.40.88610.0344-0.56190.58850.59910.06522.6378-0.0823-0.2254-0.22050.467-0.14650.54041.1597-0.14832.892471.2805-204.6603-82.1986
1350.6670.9226-1.77541.2843-2.39184.45940.9712-1.27642.12821.17550.35841.4472-1.3444-0.5538-0.55180.6323-0.04240.33080.8744-0.68372.233581.6105-204.0125-83.3212
1364.92710.6437-2.68723.9269-1.52354.2318-0.0911.48712.3936-0.4910.48122.1527-0.4468-0.5634-0.60220.7248-0.0791-0.20480.91160.37011.870278.8779-207.1556-95.2854
1375.23011.5068-3.12562.9788-0.99352.41450.4699-0.61632.20.65860.13862.1432-0.7056-0.2545-0.53730.6349-0.16280.24780.8646-0.29532.288979.8888-205.0635-86.2328
1380.6208-0.18270.37280.111-0.14670.2435-0.00420.60061.1368-0.35510.33720.8659-0.4708-1.3335-0.00240.11870.02960.4081.86410.14863.457957.2432-210.6312-85.4035
1395.6585.6464-1.38486.8357-1.20725.3397-0.34280.8556-0.61221.25330.75171.5320.2722-0.8679-0.72470.9816-0.11970.45441.2714-0.07291.776949.6592-239.6465-78.598
1404.9928-0.24571.01352.0952.91434.50230.0986-0.33840.98110.4324-0.1120.8349-0.3297-0.50080.00110.8332-0.1930.24961.2386-0.01911.711652.8118-224.8542-76.485
1416.2572-0.37174.45252.0913-0.16813.161-0.58610.20750.41561.75850.06680.39750.764-2.82970.4771.3179-0.28290.47751.7574-0.45431.620255.1616-229.6995-68.8935
1421.9683-1.67880.53172.3551-0.62463.38620.1984-0.1056-0.93040.45760.99870.814-0.3114-1.2343-1.3310.5978-0.11190.06381.64930.04651.947255.8295-227.8508-80.622
1430.10630.04630.11050.0192-0.0250.14440.6725-2.25351.2556-0.18240.3146-1.1004-0.18430.0004-0.85961.4697-0.7720.26322.4018-0.00462.302346.9811-233.542-68.0815
1441.18520.84931.87942.4353-1.84038.8503-0.5031-0.21140.64321.01570.4344-0.02760.8519-2.27720.31471.54740.05410.99861.1092-0.17973.128843.2525-226.9606-74.036
1453.96580.27271.14944.78010.89292.53530.0246-0.2474-0.10450.12280.10360.08240.29410.2734-0.1240.5494-0.11680.0220.9113-0.1610.2649152.9319-194.0005-102.6533
1464.14861.64281.8561.8510.09941.47710.1324-0.6479-0.0088-0.15710.0889-0.01710.10280.2683-0.24370.6044-0.05640.01350.8133-0.15470.3719152.4387-193.4769-103.8257
1472.67351.7129-1.03620.758-0.71980.4136-0.1398-0.49030.6903-0.41160.2498-0.2007-0.0180.6265-0.23630.8087-0.31240.19371.2381-0.39440.6437176.0099-183.8074-113.4392
1482.02551.85031.25334.5448-2.74116.1494-0.39280.03030.1621-0.10420.3788-0.4981-0.4858-0.2394-0.11610.8081-0.27970.22311.2119-0.3550.7415181.0866-179.7523-115.5072
1492.73030.69221.31721.74780.51763.7977-0.1069-0.2856-0.1528-0.63931.1105-1.073-0.33570.7877-0.05491.4567-1.24630.34721.4152-1.0370.9836185.2467-177.7336-122.7014
1503.437-0.35352.7541.483-0.45212.247-0.0382-0.3046-0.2337-1.19070.3034-0.0892-0.23260.03730.32921.3893-0.42930.18841.2896-0.5730.7497185.3066-171.0167-115.5414
1514.69742.20483.02868.0114-3.96126.1770.41510.2263-0.79681.2022-1.69750.0936-0.0777-0.53571.00110.7997-0.28840.28931.0534-0.39560.902191.9165-172.733-114.4501
1525.00091.305-1.75632.2827-2.41553.3588-0.48010.4467-0.24-0.92260.3265-0.68631.21230.20240.0350.9377-0.09980.12260.6278-0.20930.4845158.8317-199.1187-128.6356
1533.9492-0.0367-2.39591.9060.70725.4677-0.18970.67850.0306-0.49330.1803-0.05220.1010.04680.00940.7978-0.26480.00390.7074-0.11920.3473149.66-195.2895-123.4956
1543.75730.3966-0.66351.18340.4343.633-0.14650.805-0.1476-0.54460.3249-0.15080.22080.0396-0.19230.8042-0.24240.07980.8024-0.21470.4409151.6143-198.1339-123.9572
1551.83621.7357-1.30052.0983-1.39090.9232-0.40720.41240.6213-0.49560.782-0.6039-0.1491.39120.25310.7683-0.27460.39191.4139-0.63611.0695183.4441-186.3756-125.0777
1560.741.1414-0.20586.2105-1.51893.4882-0.0376-0.7104-0.1015-1.39040.5571-0.12910.68511.561-0.24560.8863-0.17330.37581.3849-0.39130.8327184.2945-191.6061-126.007
1574.6656-2.7111-0.39347.49130.90714.1817-0.304-0.596-0.3208-0.57740.038-1.28540.05411.32370.13210.7601-0.18210.42351.0266-0.11581.0667188.1118-197.7415-120.1294
1586.7855-0.14380.5612.8963-0.65145.8819-0.53-2.1775-0.1539-0.21170.78020.1362-0.61990.7318-0.0141.0073-0.21690.43421.2411-0.4080.6884182.3876-187.5697-122.4301
1590.43371.8561-0.22487.645-0.97420.1095-0.133-3.9289-1.8499-0.00770.8479-0.64310.66580.496-0.36510.7328-0.11130.02742.5282-0.42191.1242196.9197-195.0656-122.9357
1604.3156-1.1218-1.48171.3168-1.07582.5048-0.4640.3649-0.62310.11110.5855-0.23910.88972.410.39531.2298-0.45910.65612.1065-0.7551.2925193.452-190.9701-130.5946
1613.95460.8393-4.90856.3281-3.3267.290.6022-0.9696-0.703-0.6857-1.42430.11690.65451.83740.46711.28030.2782-0.02061.19470.20331.692498.3942-272.8006-123.7245
1620.1163-0.13170.18880.1482-0.21250.29960.4667-0.12920.33651.1565-0.4399-0.0588-0.8060.4634-0.32831.49570.17960.16271.86510.03791.119468.7544-190.4605-52.5166
1635.84332.89950.2032.7179-0.9730.91470.53110.647-0.05810.0343-0.22881.13320.00310.84980.12511.5399-0.6761-0.39642.25050.44551.311699.1667-191.2031-145.7319
1640.1719-0.2190.25271.4969-0.7030.4498-0.60510.95210.072-0.32050.11790.0483-0.31350.15870.0781.3655-1.1896-0.40012.92340.88532.9658132.5245-218.7767-76.8178
Refinement TLS group
IDRefine-IDRefine TLS-IDSelection detailsAuth asym-IDAuth seq-ID
1X-RAY DIFFRACTION1chain 'A' and (resid 4 through 89 )A0
2X-RAY DIFFRACTION2chain 'A' and (resid 90 through 135 )A0
3X-RAY DIFFRACTION3chain 'A' and (resid 136 through 178 )A0
4X-RAY DIFFRACTION4chain 'A' and (resid 179 through 230 )A0
5X-RAY DIFFRACTION5chain 'A' and (resid 231 through 285 )A0
6X-RAY DIFFRACTION6chain 'A' and (resid 286 through 350 )A0
7X-RAY DIFFRACTION7chain 'B' and (resid 4 through 98 )B0
8X-RAY DIFFRACTION8chain 'B' and (resid 99 through 178 )B0
9X-RAY DIFFRACTION9chain 'B' and (resid 179 through 285 )B0
10X-RAY DIFFRACTION10chain 'B' and (resid 286 through 352 )B0
11X-RAY DIFFRACTION11chain 'C' and (resid 4 through 128 )C0
12X-RAY DIFFRACTION12chain 'C' and (resid 129 through 225 )C0
13X-RAY DIFFRACTION13chain 'D' and (resid 2 through 19 )D0
14X-RAY DIFFRACTION14chain 'D' and (resid 20 through 91 )D0
15X-RAY DIFFRACTION15chain 'D' and (resid 92 through 116 )D0
16X-RAY DIFFRACTION16chain 'D' and (resid 117 through 153 )D0
17X-RAY DIFFRACTION17chain 'D' and (resid 154 through 166 )D0
18X-RAY DIFFRACTION18chain 'D' and (resid 167 through 201 )D0
19X-RAY DIFFRACTION19chain 'D' and (resid 202 through 217 )D0
20X-RAY DIFFRACTION20chain 'E' and (resid 4 through 20 )E0
21X-RAY DIFFRACTION21chain 'E' and (resid 21 through 55 )E0
22X-RAY DIFFRACTION22chain 'E' and (resid 56 through 76 )E0
23X-RAY DIFFRACTION23chain 'E' and (resid 77 through 128 )E0
24X-RAY DIFFRACTION24chain 'E' and (resid 129 through 144 )E0
25X-RAY DIFFRACTION25chain 'E' and (resid 145 through 166 )E0
26X-RAY DIFFRACTION26chain 'E' and (resid 167 through 203 )E0
27X-RAY DIFFRACTION27chain 'E' and (resid 204 through 225 )E0
28X-RAY DIFFRACTION28chain 'F' and (resid 3 through 19 )F0
29X-RAY DIFFRACTION29chain 'F' and (resid 20 through 91 )F0
30X-RAY DIFFRACTION30chain 'F' and (resid 92 through 116 )F0
31X-RAY DIFFRACTION31chain 'F' and (resid 117 through 189 )F0
32X-RAY DIFFRACTION32chain 'F' and (resid 190 through 217 )F0
33X-RAY DIFFRACTION33chain 'G' and (resid 4 through 30 )G0
34X-RAY DIFFRACTION34chain 'G' and (resid 31 through 99 )G0
35X-RAY DIFFRACTION35chain 'G' and (resid 100 through 178 )G0
36X-RAY DIFFRACTION36chain 'G' and (resid 179 through 262 )G0
37X-RAY DIFFRACTION37chain 'G' and (resid 263 through 285 )G0
38X-RAY DIFFRACTION38chain 'G' and (resid 286 through 350 )G0
39X-RAY DIFFRACTION39chain 'H' and (resid 5 through 98 )H0
40X-RAY DIFFRACTION40chain 'H' and (resid 99 through 152 )H0
41X-RAY DIFFRACTION41chain 'H' and (resid 153 through 230 )H0
42X-RAY DIFFRACTION42chain 'H' and (resid 231 through 352 )H0
43X-RAY DIFFRACTION43chain 'I' and (resid 1 through 28 )I0
44X-RAY DIFFRACTION44chain 'I' and (resid 29 through 128 )I0
45X-RAY DIFFRACTION45chain 'I' and (resid 129 through 225 )I0
46X-RAY DIFFRACTION46chain 'J' and (resid 3 through 19 )J0
47X-RAY DIFFRACTION47chain 'J' and (resid 20 through 91 )J0
48X-RAY DIFFRACTION48chain 'J' and (resid 92 through 104 )J0
49X-RAY DIFFRACTION49chain 'J' and (resid 105 through 116 )J0
50X-RAY DIFFRACTION50chain 'J' and (resid 117 through 153 )J0
51X-RAY DIFFRACTION51chain 'J' and (resid 154 through 166 )J0
52X-RAY DIFFRACTION52chain 'J' and (resid 167 through 201 )J0
53X-RAY DIFFRACTION53chain 'J' and (resid 202 through 217 )J0
54X-RAY DIFFRACTION54chain 'K' and (resid 5 through 76 )K0
55X-RAY DIFFRACTION55chain 'K' and (resid 77 through 128 )K0
56X-RAY DIFFRACTION56chain 'K' and (resid 129 through 154 )K0
57X-RAY DIFFRACTION57chain 'K' and (resid 155 through 166 )K0
58X-RAY DIFFRACTION58chain 'K' and (resid 167 through 184 )K0
59X-RAY DIFFRACTION59chain 'K' and (resid 185 through 203 )K0
60X-RAY DIFFRACTION60chain 'K' and (resid 204 through 225 )K0
61X-RAY DIFFRACTION61chain 'L' and (resid 3 through 19 )L0
62X-RAY DIFFRACTION62chain 'L' and (resid 20 through 62 )L0
63X-RAY DIFFRACTION63chain 'L' and (resid 63 through 91 )L0
64X-RAY DIFFRACTION64chain 'L' and (resid 92 through 104 )L0
65X-RAY DIFFRACTION65chain 'L' and (resid 105 through 116 )L0
66X-RAY DIFFRACTION66chain 'L' and (resid 117 through 153 )L0
67X-RAY DIFFRACTION67chain 'L' and (resid 154 through 166 )L0
68X-RAY DIFFRACTION68chain 'L' and (resid 167 through 189 )L0
69X-RAY DIFFRACTION69chain 'L' and (resid 190 through 217 )L0
70X-RAY DIFFRACTION70chain 'M' and (resid 4 through 135 )M0
71X-RAY DIFFRACTION71chain 'M' and (resid 136 through 230 )M0
72X-RAY DIFFRACTION72chain 'M' and (resid 231 through 350 )M0
73X-RAY DIFFRACTION73chain 'N' and (resid 2 through 81 )N0
74X-RAY DIFFRACTION74chain 'N' and (resid 82 through 135 )N0
75X-RAY DIFFRACTION75chain 'N' and (resid 136 through 262 )N0
76X-RAY DIFFRACTION76chain 'N' and (resid 263 through 285 )N0
77X-RAY DIFFRACTION77chain 'N' and (resid 286 through 352 )N0
78X-RAY DIFFRACTION78chain 'O' and (resid 3 through 20 )O0
79X-RAY DIFFRACTION79chain 'O' and (resid 21 through 76 )O0
80X-RAY DIFFRACTION80chain 'O' and (resid 77 through 128 )O0
81X-RAY DIFFRACTION81chain 'O' and (resid 129 through 154 )O0
82X-RAY DIFFRACTION82chain 'O' and (resid 155 through 166 )O0
83X-RAY DIFFRACTION83chain 'O' and (resid 167 through 197 )O0
84X-RAY DIFFRACTION84chain 'O' and (resid 198 through 212 )O0
85X-RAY DIFFRACTION85chain 'O' and (resid 213 through 225 )O0
86X-RAY DIFFRACTION86chain 'P' and (resid 2 through 19 )P0
87X-RAY DIFFRACTION87chain 'P' and (resid 20 through 104 )P0
88X-RAY DIFFRACTION88chain 'P' and (resid 105 through 116 )P0
89X-RAY DIFFRACTION89chain 'P' and (resid 117 through 153 )P0
90X-RAY DIFFRACTION90chain 'P' and (resid 154 through 166 )P0
91X-RAY DIFFRACTION91chain 'P' and (resid 167 through 177 )P0
92X-RAY DIFFRACTION92chain 'P' and (resid 178 through 191 )P0
93X-RAY DIFFRACTION93chain 'P' and (resid 192 through 217 )P0
94X-RAY DIFFRACTION94chain 'Q' and (resid 5 through 42 )Q0
95X-RAY DIFFRACTION95chain 'Q' and (resid 43 through 76 )Q0
96X-RAY DIFFRACTION96chain 'Q' and (resid 77 through 133 )Q0
97X-RAY DIFFRACTION97chain 'Q' and (resid 134 through 144 )Q0
98X-RAY DIFFRACTION98chain 'Q' and (resid 145 through 184 )Q0
99X-RAY DIFFRACTION99chain 'Q' and (resid 185 through 203 )Q0
100X-RAY DIFFRACTION100chain 'Q' and (resid 204 through 225 )Q0
101X-RAY DIFFRACTION101chain 'R' and (resid 2 through 19 )R0
102X-RAY DIFFRACTION102chain 'R' and (resid 20 through 62 )R0
103X-RAY DIFFRACTION103chain 'R' and (resid 63 through 76 )R0
104X-RAY DIFFRACTION104chain 'R' and (resid 77 through 91 )R0
105X-RAY DIFFRACTION105chain 'R' and (resid 92 through 116 )R0
106X-RAY DIFFRACTION106chain 'R' and (resid 117 through 131 )R0
107X-RAY DIFFRACTION107chain 'R' and (resid 132 through 153 )R0
108X-RAY DIFFRACTION108chain 'R' and (resid 154 through 166 )R0
109X-RAY DIFFRACTION109chain 'R' and (resid 167 through 189 )R0
110X-RAY DIFFRACTION110chain 'R' and (resid 190 through 200 )R0
111X-RAY DIFFRACTION111chain 'R' and (resid 201 through 217 )R0
112X-RAY DIFFRACTION112chain 'S' and (resid 4 through 55 )S0
113X-RAY DIFFRACTION113chain 'S' and (resid 56 through 81 )S0
114X-RAY DIFFRACTION114chain 'S' and (resid 82 through 135 )S0
115X-RAY DIFFRACTION115chain 'S' and (resid 136 through 230 )S0
116X-RAY DIFFRACTION116chain 'S' and (resid 231 through 262 )S0
117X-RAY DIFFRACTION117chain 'S' and (resid 263 through 305 )S0
118X-RAY DIFFRACTION118chain 'S' and (resid 306 through 350 )S0
119X-RAY DIFFRACTION119chain 'T' and (resid 2 through 97 )T0
120X-RAY DIFFRACTION120chain 'T' and (resid 98 through 154 )T0
121X-RAY DIFFRACTION121chain 'T' and (resid 155 through 211 )T0
122X-RAY DIFFRACTION122chain 'T' and (resid 212 through 230 )T0
123X-RAY DIFFRACTION123chain 'T' and (resid 231 through 285 )T0
124X-RAY DIFFRACTION124chain 'T' and (resid 286 through 351 )T0
125X-RAY DIFFRACTION125chain 'U' and (resid 4 through 55 )U0
126X-RAY DIFFRACTION126chain 'U' and (resid 56 through 100 )U0
127X-RAY DIFFRACTION127chain 'U' and (resid 101 through 115 )U0
128X-RAY DIFFRACTION128chain 'U' and (resid 116 through 128 )U0
129X-RAY DIFFRACTION129chain 'U' and (resid 129 through 163 )U0
130X-RAY DIFFRACTION130chain 'U' and (resid 164 through 174 )U0
131X-RAY DIFFRACTION131chain 'U' and (resid 175 through 186 )U0
132X-RAY DIFFRACTION132chain 'U' and (resid 187 through 203 )U0
133X-RAY DIFFRACTION133chain 'U' and (resid 204 through 225 )U0
134X-RAY DIFFRACTION134chain 'V' and (resid 3 through 19 )V0
135X-RAY DIFFRACTION135chain 'V' and (resid 20 through 39 )V0
136X-RAY DIFFRACTION136chain 'V' and (resid 40 through 62 )V0
137X-RAY DIFFRACTION137chain 'V' and (resid 63 through 104 )V0
138X-RAY DIFFRACTION138chain 'V' and (resid 105 through 116 )V0
139X-RAY DIFFRACTION139chain 'V' and (resid 117 through 131 )V0
140X-RAY DIFFRACTION140chain 'V' and (resid 132 through 153 )V0
141X-RAY DIFFRACTION141chain 'V' and (resid 154 through 166 )V0
142X-RAY DIFFRACTION142chain 'V' and (resid 167 through 189 )V0
143X-RAY DIFFRACTION143chain 'V' and (resid 190 through 200 )V0
144X-RAY DIFFRACTION144chain 'V' and (resid 201 through 217 )V0
145X-RAY DIFFRACTION145chain 'W' and (resid 5 through 76 )W0
146X-RAY DIFFRACTION146chain 'W' and (resid 77 through 108 )W0
147X-RAY DIFFRACTION147chain 'W' and (resid 109 through 143 )W0
148X-RAY DIFFRACTION148chain 'W' and (resid 144 through 184 )W0
149X-RAY DIFFRACTION149chain 'W' and (resid 185 through 197 )W0
150X-RAY DIFFRACTION150chain 'W' and (resid 198 through 212 )W0
151X-RAY DIFFRACTION151chain 'W' and (resid 213 through 225 )W0
152X-RAY DIFFRACTION152chain 'X' and (resid 2 through 19 )X0
153X-RAY DIFFRACTION153chain 'X' and (resid 20 through 62 )X0
154X-RAY DIFFRACTION154chain 'X' and (resid 63 through 104 )X0
155X-RAY DIFFRACTION155chain 'X' and (resid 105 through 131 )X0
156X-RAY DIFFRACTION156chain 'X' and (resid 132 through 153 )X0
157X-RAY DIFFRACTION157chain 'X' and (resid 154 through 166 )X0
158X-RAY DIFFRACTION158chain 'X' and (resid 167 through 189 )X0
159X-RAY DIFFRACTION159chain 'X' and (resid 190 through 200 )X0
160X-RAY DIFFRACTION160chain 'X' and (resid 201 through 217 )X0
161X-RAY DIFFRACTION161chain 'a' and (resid 1 through 20 )a0
162X-RAY DIFFRACTION162chain 'g' and (resid 3 through 16 )g0
163X-RAY DIFFRACTION163chain 'm' and (resid 2 through 20 )m0
164X-RAY DIFFRACTION164chain 's' and (resid 0 through 20 )s0

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