温度: 293 K / 手法: 蒸気拡散法, シッティングドロップ法 / pH: 7 詳細: 10ul drop containing: 1ul of 4mM lambda-[Ru(TAP)2(dppz-{Me2})]2+; 1ul of 1mM d(TCGGTACCGA)2, and a 8ul solution containing 12mM spermine, 10% 2-methyl-2,4-pentanediol, 40mM sodium cacodylate ...詳細: 10ul drop containing: 1ul of 4mM lambda-[Ru(TAP)2(dppz-{Me2})]2+; 1ul of 1mM d(TCGGTACCGA)2, and a 8ul solution containing 12mM spermine, 10% 2-methyl-2,4-pentanediol, 40mM sodium cacodylate pH 7.0, 80mM NaCl and 20mM BaCl2. This was equilibrated against a 1ml reservoir of 35% 2-methyl-2,4-pantanediol., VAPOR DIFFUSION, SITTING DROP, temperature 293K
解像度: 2.05→36.93 Å / Cor.coef. Fo:Fc: 0.929 / Cor.coef. Fo:Fc free: 0.889 / SU B: 5.178 / SU ML: 0.139 / 交差検証法: THROUGHOUT / ESU R: 0.214 / ESU R Free: 0.216 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.32103
138
4.3 %
RANDOM
Rwork
0.24498
-
-
-
obs
0.24806
3048
97.82 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK