GDP-L-FUCOSESYNTHASE / GDP-4-KETO-6-DEOXY-D-MANNOSE-3 / 5-EPIMERASE-4-REDUCTASE / PROTEIN FX / RED CELL NADP(H)-BINDING ...GDP-4-KETO-6-DEOXY-D-MANNOSE-3 / 5-EPIMERASE-4-REDUCTASE / PROTEIN FX / RED CELL NADP(H)-BINDING PROTEIN / SHORT-CHAIN DEHYDROGENASE/REDUCTASE FAMILY 4E MEMBER 1
Mass: 37807.586 Da / Num. of mol.: 4 Source method: isolated from a genetically manipulated source Source: (gene. exp.) HOMO SAPIENS (human) / Plasmid: PNIC28-BSA4 / Production host: ESCHERICHIA COLI (E. coli) / Strain (production host): BL21(DE3) / Variant (production host): R3 / References: UniProt: Q13630, GDP-L-fucose synthase
Resolution: 2.7→49.44 Å / Cor.coef. Fo:Fc: 0.946 / Cor.coef. Fo:Fc free: 0.934 / SU B: 22.103 / SU ML: 0.223 / Cross valid method: THROUGHOUT / ESU R: 0.766 / ESU R Free: 0.299 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES WITH TLS ADDED
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.23091
2408
5.1 %
RANDOM
Rwork
0.19603
-
-
-
obs
0.1978
45196
99.95 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK