Resolution: 2.1→31.68 Å / Cor.coef. Fo:Fc: 0.932 / Cor.coef. Fo:Fc free: 0.917 / Cross valid method: THROUGHOUT / σ(F): 0 Details: The programs MOLPROBITY, COOT have also been used during refinement
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.226
701
4.94 %
THIN SHELLS (SFTOOLS)
Rwork
0.204
-
-
-
obs
0.205
13479
-
-
Displacement parameters
Biso mean: 32.36 Å2
Baniso -1
Baniso -2
Baniso -3
1-
-0.495 Å2
0 Å2
0 Å2
2-
-
-0.495 Å2
0 Å2
3-
-
-
0.989 Å2
Refine analyze
Luzzati coordinate error obs: 0.256 Å
Refinement step
Cycle: LAST / Resolution: 2.1→31.68 Å
Protein
Nucleic acid
Ligand
Solvent
Total
Num. atoms
1612
0
4
55
1671
LS refinement shell
Resolution: 2.1→2.27 Å / Total num. of bins used: 7
Rfactor
Num. reflection
% reflection
Rfree
0.299
124
4.77 %
Rwork
0.215
2475
-
all
0.22
2599
-
+
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