SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AA" IN EACH CHAIN ON SHEET RECORDS BELOW ... SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AA" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 13-STRANDED BARREL THIS IS REPRESENTED BY A 14-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL. THE SHEETS PRESENTED AS "BA", "CA" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 11-STRANDED BARREL THIS IS REPRESENTED BY A 12-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL. THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN THE SHEET RECORDS BELOW, TWO SHEETS ARE DEFINED.
マシュー密度: 3.34 Å3/Da / 溶媒含有率: 62.83 % 解説: THE DATA WERE COLLECTED AT ROOM TEMPERATURE, DURING CONTROLLED DEHYDRATION OF CRYSTALS,TO EVALUATE THE CHANGES THAT OCCUR IN CRYSTAL PACKING DURING DEHYDRATION. NO BIOLOGICAL SIGNIFICANCE ...解説: THE DATA WERE COLLECTED AT ROOM TEMPERATURE, DURING CONTROLLED DEHYDRATION OF CRYSTALS,TO EVALUATE THE CHANGES THAT OCCUR IN CRYSTAL PACKING DURING DEHYDRATION. NO BIOLOGICAL SIGNIFICANCE SHOULD BE ATTACHED TO THE COORDINATES.
結晶化
pH: 8.5 詳細: 50 MM TRIS-HCL PH 8.2, 200 MM NACL, 20 MM MGSO4, 1 MM ADP, 1 MM ALCL3, 6 MM NAF 0.004% (W/V)PHENYLMETHYLSULFONYL FLUORIDE AND 12% (W/V) POLYETHYLENE GLYCOL 6000
解像度: 6→30 Å / Cor.coef. Fo:Fc: 0.741 / Cor.coef. Fo:Fc free: 0.793 / SU B: 0.008 / SU ML: 0 / 交差検証法: THROUGHOUT / ESU R: 3.611 / ESU R Free: 3.591 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. THIS STRUCTURE WAS DETERMINED TO EVALUATE CHANGING CRYSTAL CONTACTS DURING CONTROLLED DEHYDRATION OF CRYSTALS. NO BIOLOGICAL SIGNIFICANCE ...詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. THIS STRUCTURE WAS DETERMINED TO EVALUATE CHANGING CRYSTAL CONTACTS DURING CONTROLLED DEHYDRATION OF CRYSTALS. NO BIOLOGICAL SIGNIFICANCE SHOULD BE ATTACHED TO THE COORDINATES.
Rfactor
反射数
%反射
Selection details
Rfree
0.343
439
4.8 %
RANDOM
Rwork
0.345
-
-
-
obs
0.345
8721
83 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK