SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN ... SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN THE SHEET RECORDS BELOW, TWO SHEETS ARE DEFINED.
ENGINEERED RESIDUE IN CHAIN A, GLU 154 TO HIS ENGINEERED RESIDUE IN CHAIN A, GLU 156 TO HIS ...ENGINEERED RESIDUE IN CHAIN A, GLU 154 TO HIS ENGINEERED RESIDUE IN CHAIN A, GLU 156 TO HIS ENGINEERED RESIDUE IN CHAIN B, GLU 154 TO HIS ENGINEERED RESIDUE IN CHAIN B, GLU 156 TO HIS
配列の詳細
MUTATIONS ENGINEERED TO FACILITATE CRYSTALLIZATION
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 4.42 Å3/Da / 溶媒含有率: 72.2 %
結晶化
pH: 7.5 / 詳細: 1.4 M SODIUM CITRATE 0.1 M HEPES PH 7.5
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データ収集
回折
平均測定温度: 100 K
放射光源
由来: シンクロトロン / サイト: APS / ビームライン: 22-BM / 波長: 1
検出器
タイプ: MARRESEARCH / 検出器: CCD / 日付: 2005年11月9日
放射
プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 1 Å / 相対比: 1
反射
解像度: 1.6→40 Å / Num. obs: 69501 / % possible obs: 99.7 % / 冗長度: 10.3 % / Rmerge(I) obs: 0.07 / Net I/σ(I): 39
反射 シェル
解像度: 1.6→1.66 Å / 冗長度: 4.9 % / Rmerge(I) obs: 0.8 / Mean I/σ(I) obs: 1.42 / % possible all: 96.5
解像度: 1.6→92.85 Å / Cor.coef. Fo:Fc: 0.959 / Cor.coef. Fo:Fc free: 0.939 / SU B: 2.309 / SU ML: 0.045 / 交差検証法: THROUGHOUT / ESU R: 0.067 / ESU R Free: 0.07 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
反射数
%反射
Selection details
Rfree
0.219
1401
2 %
RANDOM
Rwork
0.194
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obs
0.195
68064
99.5 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK