マシュー密度: 3.19 Å3/Da / 溶媒含有率: 61.49 % 解説: PHASING WAS OBTAINED FROM A MULTI-WAVELENGTH ANOMALOUS DIFFRACTION (MAD) EXPERIMENT ON A PCMBS-DERIVATIZED CRYSTAL; THE MERCURY POSITION WAS POORLY OCCUPIED (~0.2), AND SO THE DERIVED PHASES ...解説: PHASING WAS OBTAINED FROM A MULTI-WAVELENGTH ANOMALOUS DIFFRACTION (MAD) EXPERIMENT ON A PCMBS-DERIVATIZED CRYSTAL; THE MERCURY POSITION WAS POORLY OCCUPIED (~0.2), AND SO THE DERIVED PHASES WERE COMBINED WITH PHASES OBTAINED BY SIR/AS ON A MORE COMPLETELY DERIVATIZED CRYSTAL.
結晶化
*PLUS
温度: 4 ℃ / pH: 8 / 手法: 蒸気拡散法, ハンギングドロップ法
溶液の組成
*PLUS
ID
濃度
一般名
Crystal-ID
Sol-ID
化学式
1
45mg/ml
protein
1
drop
2
10mM
Tris
1
drop
3
0.3M
1
drop
NaCl
4
10mM
Tris
1
reservoir
5
1.0M
1
reservoir
NaCl
-
データ収集
放射
散乱光タイプ: x-ray
放射波長
相対比: 1
反射
*PLUS
最高解像度: 1.9 Å / Num. obs: 14552 / % possible obs: 98.2 % / Rmerge(I) obs: 0.041