SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN ... SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN THE SHEET RECORDS BELOW, TWO SHEETS ARE DEFINED.
THE SEQUENCE IS DESCRIBED IN CALVETE ET AL. (1999) BIOCHIM. BIOPHYS. ACTA., 1430, P.367. RESIDUES ...THE SEQUENCE IS DESCRIBED IN CALVETE ET AL. (1999) BIOCHIM. BIOPHYS. ACTA., 1430, P.367. RESIDUES 144 AND 190 (GLY AND SER) ARE NOT SET CORRECTLY IN THE SW DATA BASE.
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2.11 Å3/Da / 溶媒含有率: 41.3 %
結晶化
手法: 蒸気拡散法, ハンギングドロップ法 / pH: 4.6 詳細: CRYSTALS WERE GROWN BY THE HANGING DROP VAPOUR DIFFUSION METHOD USING 30% PEG 400, 0.1M ACO, PH 4.6, 10MM CACL2 AND MNCL2
解像度: 2→22.54 Å / Rfactor Rfree error: 0.006 / Data cutoff high absF: 2397478.65 / Isotropic thermal model: RESTRAINED / 交差検証法: THROUGHOUT / σ(F): 0 詳細: SIDE-CHAINS COULD NOT BE ADDED FOR RESIDUES A131, A162, A204, B82, B99 AND B116, AND RESIDUES WERE NOT BUILT FOR B117 AND B237 BECAUSE OF THE LACK OF DENSITY THE RESIDUES 118-122 WERE LEFT ...詳細: SIDE-CHAINS COULD NOT BE ADDED FOR RESIDUES A131, A162, A204, B82, B99 AND B116, AND RESIDUES WERE NOT BUILT FOR B117 AND B237 BECAUSE OF THE LACK OF DENSITY THE RESIDUES 118-122 WERE LEFT OUT FOR BOTH MONOMERS BECAUSE OF POOR DENSITY. THE C-TERMINAL RESIDUE ASN237 WAS NOT SEEN IN THE DENSITY MAPS