8V61
UIC-1 mutant - UIC-1-L6I
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-23 |
Detector | RIGAKU HyPix-3000 |
Wavelength(s) | 1.54184 |
Spacegroup name | P 1 |
Unit cell lengths | 10.311, 28.251, 32.535 |
Unit cell angles | 111.07, 90.26, 90.28 |
Refinement procedure
Resolution | 15.850 - 1.130 |
R-factor | 0.1862 |
Rwork | 0.184 |
R-free | 0.20790 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.814 |
Data reduction software | CrysalisPro |
Data scaling software | CrysalisPro |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.850 | 1.170 |
High resolution limit [Å] | 1.130 | 1.130 |
Rmerge | 0.053 | 0.841 |
Rmeas | 0.058 | 0.978 |
Number of reflections | 12284 | 1104 |
<I/σ(I)> | 16.88 | 1.28 |
Completeness [%] | 95.2 | 86.61 |
Redundancy | 4.9 | 3.6 |
CC(1/2) | 0.999 | 0.817 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SLOW COOLING | 298 | water, acetonitrile |