8OV7
Crystal structure of D1228V c-MET bound by compound 10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 111.645, 111.645, 130.432 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.270 - 1.950 |
R-factor | 0.2737 |
Rwork | 0.273 |
R-free | 0.28700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.900 |
Data reduction software | DIALS |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.8 (8-JUN-2022)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.940 | 1.980 |
High resolution limit [Å] | 1.950 | 1.950 |
Number of reflections | 60639 | 2948 |
<I/σ(I)> | 9.6 | |
Completeness [%] | 100.0 | |
Redundancy | 12.5 | |
CC(1/2) | 0.998 | 0.512 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 1.5 M LiCl, 0.1 M Na HEPES pH 7.5 |