8IDX
Structure of p205 HIN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-01-01 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.979150 |
| Spacegroup name | P 1 |
| Unit cell lengths | 48.638, 51.121, 56.578 |
| Unit cell angles | 103.15, 105.17, 108.29 |
Refinement procedure
| Resolution | 29.546 - 1.750 |
| R-factor | 0.1738 |
| Rwork | 0.172 |
| R-free | 0.19880 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.765 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.15_3459: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.546 | 1.813 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Rmerge | 0.023 | 0.250 |
| Rmeas | 0.027 | 0.299 |
| Rpim | 0.014 | |
| Number of reflections | 158200 | 15198 |
| <I/σ(I)> | 28.96 | |
| Completeness [%] | 95.3 | 94.55 |
| Redundancy | 3.5 | 3.4 |
| CC(1/2) | 1.000 | 0.969 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 9 | 289 | 0.1 M Sodium chloride, 0.1 M BICINE pH 9.0, 25% v/v Polyethylene glycol monomethyl ether 550 |
