7YQP
Xcc Nicotinamide Phosphoribosyltransferase
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-12 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979183 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 115.898, 115.898, 160.113 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 54.490 - 2.088 |
R-factor | 0.2211 |
Rwork | 0.218 |
R-free | 0.25260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7yqo |
Data reduction software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.15_3459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.620 | 9.300 |
High resolution limit [Å] | 2.080 | 2.080 |
Number of reflections | 25813 | 2831 |
<I/σ(I)> | 21.8 | |
Completeness [%] | 100.0 | |
Redundancy | 14.05 | |
CC(1/2) | 1.000 | 0.900 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | ammonium tartrate, N,N-Bis(3-D-gluconamidopropyl) cholamide, N,N-Dimethyldecylamine-N-oxide |