7R96
Self-Assembled 3D DNA Hexagonal Tensegrity Triangle
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-11-14 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.60648 |
Spacegroup name | P 63 |
Unit cell lengths | 125.206, 125.206, 65.227 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 54.220 - 5.680 |
Rwork | 0.120 |
R-free | 0.14300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3gbi |
RMSD bond length | 0.005 |
RMSD bond angle | 0.765 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 54.220 | 55.893 | 6.354 |
High resolution limit [Å] | 5.680 | 11.831 | 5.683 |
Rmerge | 0.187 | ||
Rmeas | 0.193 | ||
Rpim | 0.045 | ||
Number of reflections | 1486 | 211 | 216 |
<I/σ(I)> | 11.2 | 0.9 | |
Completeness [%] | 89.1 | 100 | 57.4 |
Redundancy | 19.4 | 17.9 | 17.7 |
CC(1/2) | 0.996 | 0.996 | 0.054 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.5 | 293 | Ammonium sulfate, Tris, Acetic Acid, EDTA, Cobalt Hexammine |