Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-02-07 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.680, 88.420, 97.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.704 - 2.060 |
Rwork | 0.218 |
R-free | 0.23610 |
Structure solution method | MIR |
RMSD bond length | 0.004 |
RMSD bond angle | 1.081 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.704 | 2.110 |
High resolution limit [Å] | 2.060 | 2.060 |
Number of reflections | 32047 | 2323 |
<I/σ(I)> | 14.93 | |
Completeness [%] | 100.0 | |
Redundancy | 12.8 | |
CC(1/2) | 0.990 | 0.540 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.9 | 293 | 10% PEG 20 000, 25% PEG MME 550, 0.1 M MES/imidazole, pH 6.9, 0.03 M NaNO3, 0.03 M Na2HPO4, 0.03 M (NH4)2SO |