7Q6I
Vibrio maritimus FtsA 1-396 ATP and FtsN 1-29, bent tetramers in double filament arrangement
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-09-15 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 1.00915 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 98.692, 119.993, 329.788 |
Unit cell angles | 90.00, 93.76, 90.00 |
Refinement procedure
Resolution | 49.880 - 3.600 |
R-factor | 0.2428 |
Rwork | 0.241 |
R-free | 0.28700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7q6f |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER |
Refinement software | PHENIX (1.20rc1_4392) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 75.980 | 75.980 | 3.690 |
High resolution limit [Å] | 3.600 | 16.100 | 3.600 |
Rmerge | 0.163 | 0.049 | 1.197 |
Rmeas | 0.177 | 0.053 | 1.294 |
Rpim | 0.067 | 0.020 | 0.489 |
Total number of observations | 620636 | 7006 | 46750 |
Number of reflections | 89730 | 1072 | 6579 |
<I/σ(I)> | 8.6 | 23 | 1.8 |
Completeness [%] | 100.0 | 98.9 | 100 |
Redundancy | 6.9 | 6.5 | 7.1 |
CC(1/2) | 0.997 | 0.997 | 0.983 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294.15 | 21.645 % v/v PEG 600, 0.125 M MgCl2, 0.1 M Tris/HCl pH 8.5 |