7JKB
2xVH Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 70.480, 195.000, 91.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.750 - 2.550 |
R-factor | 0.2578 |
Rwork | 0.254 |
R-free | 0.29160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | modeled Fab |
Data reduction software | xia2 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3211) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.750 | 48.750 | 2.620 |
High resolution limit [Å] | 2.550 | 11.400 | 2.550 |
Rmerge | 0.054 | 0.028 | 1.044 |
Number of reflections | 20965 | 276 | 2042 |
<I/σ(I)> | 18.8 | ||
Completeness [%] | 99.9 | 98.6 | 99.9 |
Redundancy | 6.6 | 5.2 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 1M lithium chloride, 0.1M citric acid pH 4.0 |