7FDZ
Levansucrase from Brenneria sp. EniD 312 with sucrose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-08-07 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 98.125, 98.125, 215.534 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 84.980 - 1.350 |
R-factor | 0.1301 |
Rwork | 0.129 |
R-free | 0.14980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4d47 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.545 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.980 | 1.200 |
High resolution limit [Å] | 1.180 | 1.180 |
Number of reflections | 161790 | 578 |
<I/σ(I)> | 18.8 | |
Completeness [%] | 80.7 | 5.9 |
Redundancy | 38.1 | |
CC(1/2) | 1.000 | 0.644 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | Ammonium sulfate, PEG 400 |