7DKI
Silk worm FKBP, isoform-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 193.15 |
Detector technology | PIXEL |
Collection date | 2019-01-14 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 32 |
Unit cell lengths | 52.409, 52.409, 77.109 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.388 - 2.000 |
R-factor | 0.1592 |
Rwork | 0.155 |
R-free | 0.19780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1fkb |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3247) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 5.430 | 2.000 |
Rmerge | 0.099 | 0.050 | 0.445 |
Rmeas | 0.111 | 0.056 | 0.531 |
Rpim | 0.050 | 0.025 | 0.286 |
Total number of observations | 74774 | ||
Number of reflections | 16023 | 811 | 802 |
<I/σ(I)> | 4 | ||
Completeness [%] | 100.0 | 100 | 99.8 |
Redundancy | 4.7 | 5.2 | 3.2 |
CC(1/2) | 0.998 | 0.823 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 1M sodium citrate tribasic dihydrate, 0.1M sodium cacodylate pH 6.5 |