7DH8
Crystal structure of holo XcZur
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2020-01-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 34.560, 122.900, 86.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.571 - 1.850 |
R-factor | 0.2166 |
Rwork | 0.213 |
R-free | 0.25170 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.15_3459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.571 | 1.920 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.040 | |
Rmeas | 0.529 | |
Number of reflections | 186417 | 15557 |
<I/σ(I)> | 15.35 | |
Completeness [%] | 95.5 | |
Redundancy | 11.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.2 M Sodium malonate pH 5.0, 20% w/v Polyethylene glycol 3,350 |