7BCZ
Structure of the 4'-phosphopantetheinyl transferase PcpS from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-06 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979070 |
Spacegroup name | P 1 |
Unit cell lengths | 44.359, 78.872, 81.123 |
Unit cell angles | 85.62, 84.62, 73.86 |
Refinement procedure
Resolution | 42.490 - 2.400 |
R-factor | 0.2117 |
Rwork | 0.210 |
R-free | 0.26190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6qyf |
RMSD bond length | 0.004 |
RMSD bond angle | 0.724 |
Data reduction software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.17.1_3660: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.490 | 2.486 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 39884 | 3949 |
<I/σ(I)> | 9.39 | |
Completeness [%] | 97.1 | |
Redundancy | 5.3 | |
CC(1/2) | 0.994 | 0.784 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 285 | 0.1 M Na Citrate 10 % PEG4000 10% propanol |