6ZPF
Racemic compound of RNA duplexes.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.283 |
Spacegroup name | P 1 |
Unit cell lengths | 20.850, 26.500, 38.570 |
Unit cell angles | 106.11, 96.00, 92.72 |
Refinement procedure
Resolution | 36.776 - 1.442 |
Rwork | 0.201 |
R-free | 0.24970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6zq9 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.673 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.530 |
High resolution limit [Å] | 1.440 | 1.440 |
Rmerge | 0.052 | 0.293 |
Rmeas | 0.061 | 0.343 |
Number of reflections | 12417 | 5931 |
<I/σ(I)> | 11.04 | 2.49 |
Completeness [%] | 87.3 | 74.2 |
Redundancy | 3.5 | 3.5 |
CC(1/2) | 0.999 | 0.963 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.2 M zinc acetate, 0.1 M cacodylate buffer, 18% w/v polyethylene glycol 8000 |