Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-02-22 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.0722 |
| Spacegroup name | F 41 3 2 |
| Unit cell lengths | 158.477, 158.477, 158.477 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.620 - 2.800 |
| R-factor | 0.2345 |
| Rwork | 0.232 |
| R-free | 0.27370 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6zm9 |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.460 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.620 | 2.950 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmeas | 0.125 | 0.939 |
| Number of reflections | 4409 | 634 |
| <I/σ(I)> | 9.6 | 1.8 |
| Completeness [%] | 97.7 | 98.5 |
| Redundancy | 5.2 | 5.3 |
| CC(1/2) | 0.993 | 0.610 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.5 M ammonium phosphate |
