6ZDX
RIFIN variable region bound to LILRB1 ectodomain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-29 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97857 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 134.507, 134.507, 277.468 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 277.470 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 30613 | 4346 |
<I/σ(I)> | 9.4 | |
Completeness [%] | 100.0 | |
Redundancy | 19.7 | |
CC(1/2) | 0.990 | 0.760 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 200 mM ammonium acetate, 100 mM HEPES pH 7.5, 25 % v/v isopropanol |