Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E+ SUPERBRIGHT |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2017-11-10 |
| Detector | RIGAKU SATURN A200 |
| Wavelength(s) | 1.54178 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 43.968, 48.286, 61.245 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 37.919 - 1.624 |
| Rwork | 0.183 |
| R-free | 0.22460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | in house structure |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.213 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 37.920 | 1.710 |
| High resolution limit [Å] | 1.620 | 1.620 |
| Rmerge | 0.041 | 0.331 |
| Number of reflections | 15543 | 1831 |
| <I/σ(I)> | 17.5 | 2.7 |
| Completeness [%] | 91.7 | 76.2 |
| Redundancy | 2.7 | 1.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 0.1M MES pH 6.5, 15% v/v PEG400 |
