6YDE
X-ray structure of LPMO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-27 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.90 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 39.550, 124.370, 51.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.200 |
R-factor | 0.19751 |
Rwork | 0.194 |
R-free | 0.26356 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ach |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (v5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.260 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 13174 | 977 |
<I/σ(I)> | 5.03 | |
Completeness [%] | 96.9 | |
Redundancy | 5.41 | |
CC(1/2) | 0.982 | 0.620 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289.15 | 0.1 M NaCl, 0.1 M Bis-Tris pH 6.5, 1.4 M (NH4)2SO4 |