6XDJ
Crystal Structure Analysis of MBP-SIN3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-11-12 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 79.730, 144.860, 97.090 |
Unit cell angles | 90.00, 107.97, 90.00 |
Refinement procedure
Resolution | 75.841 - 2.200 |
R-factor | 0.2074 |
Rwork | 0.206 |
R-free | 0.23990 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4jbz |
RMSD bond length | 0.003 |
RMSD bond angle | 0.582 |
Data reduction software | XDS |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 75.841 | 75.890 | 2.240 |
High resolution limit [Å] | 2.200 | 5.970 | 2.200 |
Rmeas | 0.117 | 0.043 | 1.371 |
Rpim | 0.062 | 0.023 | 0.734 |
Total number of observations | 18191 | 17750 | |
Number of reflections | 105169 | 5345 | 5224 |
<I/σ(I)> | 7.8 | 22.8 | 1 |
Completeness [%] | 99.1 | 98.7 | 99 |
Redundancy | 3.5 | 3.4 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M Bis-Tris, pH 6.0, 1.6M Ammonium sulfate |